High-yield nitration of benzene in the synthesis of 15N-labelled nitrobenzene, acetanilide, and diphenylamine

High-yield nitration of benzene in the synthesis of 15N-labelled nitrobenzene, acetanilide, and diphenylamine

Labelled H15NO3 was used as the least‐cost source of nitrogen label to prepare nitrobenzene by reaction of acetyl nitrate with excess benzene. This labelled product was subsequently converted to acetanilide‐15N and diphenylamine‐15N.

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Veröffentlicht in:Journal of labelled compounds & radiopharmaceuticals 1990-11, Vol.28 (11), p.1243-1245
Hauptverfasser: Konior, Raymond J., Yang, Ling, Walter, Robert I.
Format: Artikel
Sprache:eng
Schlagworte:
acetanilide-15N
acetyl nitrate
diphenylamine-15N
nitrobenzene-15N
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container_end_page 1245
container_issue 11
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container_title Journal of labelled compounds & radiopharmaceuticals
container_volume 28
creator Konior, Raymond J.
Yang, Ling
Walter, Robert I.
description Labelled H15NO3 was used as the least‐cost source of nitrogen label to prepare nitrobenzene by reaction of acetyl nitrate with excess benzene. This labelled product was subsequently converted to acetanilide‐15N and diphenylamine‐15N.
doi_str_mv 10.1002/jlcr.2580281103
format Article
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1099-1344
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subjects acetanilide-15N
acetyl nitrate
diphenylamine-15N
nitrobenzene-15N
title High-yield nitration of benzene in the synthesis of 15N-labelled nitrobenzene, acetanilide, and diphenylamine
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