High-yield nitration of benzene in the synthesis of 15N-labelled nitrobenzene, acetanilide, and diphenylamine

High-yield nitration of benzene in the synthesis of 15N-labelled nitrobenzene, acetanilide, and diphenylamine

Labelled H15NO3 was used as the least‐cost source of nitrogen label to prepare nitrobenzene by reaction of acetyl nitrate with excess benzene. This labelled product was subsequently converted to acetanilide‐15N and diphenylamine‐15N.

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Bibliographische Detailangaben
Veröffentlicht in:Journal of labelled compounds & radiopharmaceuticals 1990-11, Vol.28 (11), p.1243-1245
Hauptverfasser: Konior, Raymond J., Yang, Ling, Walter, Robert I.
Format: Artikel
Sprache:eng
Schlagworte:
acetanilide-15N
acetyl nitrate
diphenylamine-15N
nitrobenzene-15N
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Beschreibung
Zusammenfassung:Labelled H15NO3 was used as the least‐cost source of nitrogen label to prepare nitrobenzene by reaction of acetyl nitrate with excess benzene. This labelled product was subsequently converted to acetanilide‐15N and diphenylamine‐15N.
ISSN:0362-4803
1099-1344
DOI:10.1002/jlcr.2580281103