SIMULTANEOUS MICRODETERMINATION OF CARBON, HYDROGEN AND LEAD IN ORGANOLEAD COMPOUNDS

The straight emtpy-tube method of Korshun and Klimova has been successfully extended to the simultaneous microdetermination of carbon, hydrogen and lead in organolead compounds. In all cases, the lead content was calculated from the weight of the plumbous oxide residue left behind in the fused-silic...

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Veröffentlicht in:	Mikrochimica acta (1966) 1992-01, Vol.107 (1-2), p.37-40
Hauptverfasser:	HASSAN, HNA, HASSOUNA, MEM, GAWARGIOUS, YA
Format:	Artikel
Sprache:	eng
Schlagworte:	Analytical chemistry Chemical and thermal methods Chemistry Chemistry, Analytical Exact sciences and technology Physical Sciences Science & Technology
Online-Zugang:	Volltext
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Beschreibung
Zusammenfassung:	The straight emtpy-tube method of Korshun and Klimova has been successfully extended to the simultaneous microdetermination of carbon, hydrogen and lead in organolead compounds. In all cases, the lead content was calculated from the weight of the plumbous oxide residue left behind in the fused-silica capsule used to hold the sample. Sulphur could also be determined in the same analysis. Satisfactory results were obtained for all compounds with a standard deviation not exceeding 0.1%.
ISSN:	0026-3672 1436-5073
DOI:	10.1007/BF01772351