A new phytoecdysteroid from the stem bark ofVitex cienkowskii

To investigate differences in the metabolome of the stem bark ofVitex cienkowskiiharvested at three different locations and three different seasons, their extracts were analyzed by means of UPLC-ESI-IMS-TOF MSe. One marker metabolite was isolated and chemically characterized, which was identified as...

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Veröffentlicht in:European food research & technology 2020-12, Vol.246 (12), p.2485-2491
Hauptverfasser: Stark, Timo D., Rami, Julius, Froehlich, Sonja, Weiss, Patrick, Vierling, Wolfgang, Dongmo, Alain B., Hofmann, Thomas
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Sprache:eng
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Zusammenfassung:To investigate differences in the metabolome of the stem bark ofVitex cienkowskiiharvested at three different locations and three different seasons, their extracts were analyzed by means of UPLC-ESI-IMS-TOF MSe. One marker metabolite was isolated and chemically characterized, which was identified as the new compound 20,24-dihydroxy,24-hydroxymethylecdysone (1). IMS showed two drift time species for1which could be used as new and additional characteristic compound parameters in compound identification to reduce dereplication and false positives.
ISSN:1438-2377
1438-2385
DOI:10.1007/s00217-020-03591-z