Microstructure and wear behavior of Mo–60Si–5B coating doped with 0.5 ​at% La by spark plasma sintering

Mo–60Si–5B coating doped with 0.5 ​at% La was prepared on niobium silicon based alloy by spark plasma sintering. The microstructure and wear behavior of the 0.5La–Mo–60Si–5B (0.5La-MSB) coating were investigated. The results show that the mean grain sizes of the Mo–60Si–5B (0La-MSB) and 0.5La-MSB co...

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Veröffentlicht in:Progress in natural science 2022-12, Vol.32 (6), p.752-757
Hauptverfasser: Wu, Zilong, Feng, Kanglu, Sha, Jiangbo, Zhou, Chungen
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Sprache:eng
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Zusammenfassung:Mo–60Si–5B coating doped with 0.5 ​at% La was prepared on niobium silicon based alloy by spark plasma sintering. The microstructure and wear behavior of the 0.5La–Mo–60Si–5B (0.5La-MSB) coating were investigated. The results show that the mean grain sizes of the Mo–60Si–5B (0La-MSB) and 0.5La-MSB coatings are calculated to be 3.27 ​μm and 2.85 ​μm, respectively. The addition of La plays a role of refining the grains of 0.5La-MSB coating. The specific wear rate of 0.5La-MSB coating is decreased by up to 26.8% at the oscillation frequency of 20 ​Hz and the sliding load of 11 ​N compared to 0La-MSB coating. The anti-friction performance of Mo–60Si–5B coating is modified by the addition of 0.5 ​at.% La. The improvement of anti-friction performance of the Mo–60Si–5B coating is due to the increased hardness and the provided lubrication function by La2O3. [Display omitted] •Mo–60Si–5B coating doped with 0.5 ​at% La was deposited on Nb–Si based alloy by spark plasma sintering.•The La2O3 is observed on the grain boundary of 0.5La-MSB coating and refines the grains of 0.5La-MSB coating.•The wear resistance of Mo–60Si–5B coating is modified by the addition of 0.5 ​at.% La.•The improvement in wear resistance of the coating is attributed to the increased hardness of the alloy and the provided lubrication function by La2O3.
ISSN:1002-0071
DOI:10.1016/j.pnsc.2022.09.011