Separation of gibberellin A4 from A4 and A7 mixture by selective complex

Gibberellin A4 is effectively separated from mixture of gibberellin A4 and its analogue gibberellin A7, in the form of its crystalline complex with N,N,N',N'-tetramethylethylenediamine. After removing the tetramethylethylenediamine from the crystal by dilute HCI, gibberellin A4 is obtained a purity...

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Veröffentlicht in:Chinese chemical letters 2010-10, Vol.21 (10), p.1206-1208
Hauptverfasser: Hu, Lai Wen, Zhang, Yong Yao, Guo, Yun, Wang, Cong, Jin, Zhi Min
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Sprache:eng
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Zusammenfassung:Gibberellin A4 is effectively separated from mixture of gibberellin A4 and its analogue gibberellin A7, in the form of its crystalline complex with N,N,N',N'-tetramethylethylenediamine. After removing the tetramethylethylenediamine from the crystal by dilute HCI, gibberellin A4 is obtained a purity of 98.1% and a yield of 72.7%.
ISSN:1001-8417
1878-5964
DOI:10.1016/j.cclet.2010.05.034