Synthesis and application of an IL-supported diol as protecting group for aldehydes
A new IL-supported diol, 1-(2,3-dihydroxypropyl)-3-methylimidazolium hexafluorophosphate has been synthesized and characterized by FT-IR, 1H NMR, 13C NMR and MS (ESI). Its physical properties such as freezing point, solubility and specific gravity and thermal stability were determined. Synthetic uti...
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Veröffentlicht in: | Chinese chemical letters 2007-10, Vol.18 (10), p.1205-1208 |
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creator | Cai, Yue Qin Liu, Ye Gao, Guo Hua |
description | A new IL-supported diol, 1-(2,3-dihydroxypropyl)-3-methylimidazolium hexafluorophosphate has been synthesized and characterized by FT-IR,
1H NMR,
13C NMR and MS (ESI). Its physical properties such as freezing point, solubility and specific gravity and thermal stability were determined. Synthetic utilities of the resultant diol as a protecting group for aldehydes were also investigated. |
doi_str_mv | 10.1016/j.cclet.2007.07.012 |
format | Article |
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1H NMR,
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1H NMR,
13C NMR and MS (ESI). Its physical properties such as freezing point, solubility and specific gravity and thermal stability were determined. Synthetic utilities of the resultant diol as a protecting group for aldehydes were also investigated.</description><subject>Characterization</subject><subject>IL-supported diol</subject><subject>Preparation</subject><subject>Protecting group</subject><issn>1001-8417</issn><issn>1878-5964</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNp9UMtOwzAQjBBIlMIXcPGNU8raThz3wAEhHpUqcSicLcd2UodgR3YKlK_HoZyRRtrV7syuZrLsEsMCA2bX3UKp3owLAlAtJmBylM0wr3heLllxnHoAnPMCV6fZWYwdAOGcslm22ezduDXRRiSdRnIYeqvkaL1DvkkjtFrncTcMPoxGI219j2REQ_CjUaN1LWqD3w2o8QHJXpvtXpt4np00so_m4q_Os9eH-5e7p3z9_Li6u13nitJyzAnTStasNKReYs2oJAQ0NrKkQCWkbcl5ReuaKsyKhgOUBHilNbCCFXXD6Ty7Otz9lK6RrhWd3wWXPorvdvv1Vk9pTL5pYtIDUwUfYzCNGIJ9l2EvMIgpQdGJ3wTFpBETMEmqm4PKJBMf1gQRlTVOGW1Dci-0t__qfwDFHnpx</recordid><startdate>20071001</startdate><enddate>20071001</enddate><creator>Cai, Yue Qin</creator><creator>Liu, Ye</creator><creator>Gao, Guo Hua</creator><general>Elsevier B.V</general><general>Shanghai Key Laboratory of Green Chemistry and Chemical Processes, East China Normal University, Shanghai 200062, China</general><scope>AAYXX</scope><scope>CITATION</scope><scope>2B.</scope><scope>4A8</scope><scope>92I</scope><scope>93N</scope><scope>PSX</scope><scope>TCJ</scope></search><sort><creationdate>20071001</creationdate><title>Synthesis and application of an IL-supported diol as protecting group for aldehydes</title><author>Cai, Yue Qin ; Liu, Ye ; Gao, Guo Hua</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c335t-26dcab65e2b91d63a220d1ea5303a026d58873bb3c164f80052087dd06464bf83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>Characterization</topic><topic>IL-supported diol</topic><topic>Preparation</topic><topic>Protecting group</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Cai, Yue Qin</creatorcontrib><creatorcontrib>Liu, Ye</creatorcontrib><creatorcontrib>Gao, Guo Hua</creatorcontrib><collection>CrossRef</collection><collection>Wanfang Data Journals - Hong Kong</collection><collection>WANFANG Data Centre</collection><collection>Wanfang Data Journals</collection><collection>万方数据期刊 - 香港版</collection><collection>China Online Journals (COJ)</collection><collection>China Online Journals (COJ)</collection><jtitle>Chinese chemical letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Cai, Yue Qin</au><au>Liu, Ye</au><au>Gao, Guo Hua</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and application of an IL-supported diol as protecting group for aldehydes</atitle><jtitle>Chinese chemical letters</jtitle><date>2007-10-01</date><risdate>2007</risdate><volume>18</volume><issue>10</issue><spage>1205</spage><epage>1208</epage><pages>1205-1208</pages><issn>1001-8417</issn><eissn>1878-5964</eissn><abstract>A new IL-supported diol, 1-(2,3-dihydroxypropyl)-3-methylimidazolium hexafluorophosphate has been synthesized and characterized by FT-IR,
1H NMR,
13C NMR and MS (ESI). Its physical properties such as freezing point, solubility and specific gravity and thermal stability were determined. Synthetic utilities of the resultant diol as a protecting group for aldehydes were also investigated.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.cclet.2007.07.012</doi><tpages>4</tpages></addata></record> |
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subjects | Characterization IL-supported diol Preparation Protecting group |
title | Synthesis and application of an IL-supported diol as protecting group for aldehydes |
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