Synthesis and application of an IL-supported diol as protecting group for aldehydes

Synthesis and application of an IL-supported diol as protecting group for aldehydes

A new IL-supported diol, 1-(2,3-dihydroxypropyl)-3-methylimidazolium hexafluorophosphate has been synthesized and characterized by FT-IR, 1H NMR, 13C NMR and MS (ESI). Its physical properties such as freezing point, solubility and specific gravity and thermal stability were determined. Synthetic uti...

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Veröffentlicht in:Chinese chemical letters 2007-10, Vol.18 (10), p.1205-1208
Hauptverfasser: Cai, Yue Qin, Liu, Ye, Gao, Guo Hua
Format: Artikel
Sprache:eng
Schlagworte:
Characterization
IL-supported diol
Preparation
Protecting group
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Beschreibung
Zusammenfassung:A new IL-supported diol, 1-(2,3-dihydroxypropyl)-3-methylimidazolium hexafluorophosphate has been synthesized and characterized by FT-IR, 1H NMR, 13C NMR and MS (ESI). Its physical properties such as freezing point, solubility and specific gravity and thermal stability were determined. Synthetic utilities of the resultant diol as a protecting group for aldehydes were also investigated.
ISSN:1001-8417
1878-5964
DOI:10.1016/j.cclet.2007.07.012