Study on Drying Process of 3Al2O3·2SiO2 Mullite Gel
TQ028.6%TQ343.41; Monophasic mullite gel with composition 3Al2Q3·2SiO2 was prepared by the sol-gel method using aluminium nitrate nonahydrate, aluminium-tri-isopropoxide, and tetraethylorthosili-cate as reagents.Gels with different drying control chemical additives ( DCCAs ) and polyvinylpyrrolidone...
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| Veröffentlicht in: | 东华大学学报（英文版） 2008, Vol.25 (6), p.616-620 |
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| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Online-Zugang: | Volltext |
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| Zusammenfassung: | TQ028.6%TQ343.41; Monophasic mullite gel with composition 3Al2Q3·2SiO2 was prepared by the sol-gel method using aluminium nitrate nonahydrate, aluminium-tri-isopropoxide, and tetraethylorthosili-cate as reagents.Gels with different drying control chemical additives ( DCCAs ) and polyvinylpyrrolidone(PVP) as spinning assistant were dried at several temperatures.The influences of temperature.DCCAs and PVP in the drying process were investigated.N, N-dimethylformamide(DMF) was the optimum DCCA at 70℃ in the drying process.PVP decreased the solvent volatilization speed and prevented gel crack to a certain extent.FTIR results revealed that free water, ethanol, and isopropanol were completely removed by the drying procedure. |
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| ISSN: | 1672-5220 |