Method for producing an aqueous hydroxylamine solution devoid of salt

+++A process for preparing a salt-free aqueous hydroxylamine solution by reacting an aqueous solution of a hydroxylammonium salt with a base to give a mixture and separating from said mixture by distillation a salt-free aqueous hydroxylamine solution, involving using as a base an aqueous solution of...

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Hauptverfasser: Wostbrock, Karl-Heinz, Ströfer, Eckhard, Weber, Markus, Kerth, Steffen
Format: Patent
Sprache:eng
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Zusammenfassung:+++A process for preparing a salt-free aqueous hydroxylamine solution by reacting an aqueous solution of a hydroxylammonium salt with a base to give a mixture and separating from said mixture by distillation a salt-free aqueous hydroxylamine solution, involving using as a base an aqueous solution of a mixture of NaOH and KOH in a molar ratio Na:K in the range from 70:30 to 95:5 and with a total concentration of Na and K in the range from 0.1 to 10 m/m % based on the total amount of the mixture.