Device for solvent extraction in a microwave field
The invention relates to apparatus for extracting solvents in a microwave field, having a microwave oven ( 11 ) which comprises at least one microwave generator ( 12 ), a control unit ( 13 ) and at least one microwaving chamber ( 14 ), said chamber being fitted with venting apertures ( 23 ) and at l...
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Format: | Patent |
Sprache: | eng |
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Zusammenfassung: | The invention relates to apparatus for extracting solvents in a microwave field, having a microwave oven (
11
) which comprises at least one microwave generator (
12
), a control unit (
13
) and at least one microwaving chamber (
14
), said chamber being fitted with venting apertures (
23
) and at least one suction exhaust aperture (
24
) which is connected by an exhaust air line (
25
) to a source of partial vacuum (
26
), further comprising a rotor (
16
) rotatably mounted in said chamber and fitted with several specimen receptacles (
18
) that may be loaded with solvent. The apparatus is characterized in that a flow detector (
28
) is mounted downstream of the suction exhaust aperture (
24
), said detector reducing or preferably shutting off the power output of the microwave generator (
12
) when detecting a flow of air which is less than a predetermined limit value, said airflow limit value being selected in a manner precluding forming an explosive mixture of solvent and air in said chamber. Preferably the specimen receptacles (
18
) are designed as pressure-resistant receptacles advantageously fitted with throttled overpressure valves (
35
). |
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