Method for producing an aqueous hydroxylamine solution devoid of salt

A process for preparing a salt-free aqueous hydroxylamine solution by reacting an aqueous solution of a hydroxylammonium salt with a base to give a mixture and separating from said mixture by distillation a salt-free aqueous hydroxylamine solution, comprises using as a base an aqueous solution of a...

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Bibliographische Detailangaben
Hauptverfasser: Strofer, Eckhard, Wostbrock, Karl-Heinz, Weber, Markus, Kerth, Steffen
Format: Patent
Sprache:eng
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Zusammenfassung:A process for preparing a salt-free aqueous hydroxylamine solution by reacting an aqueous solution of a hydroxylammonium salt with a base to give a mixture and separating from said mixture by distillation a salt-free aqueous hydroxylamine solution, comprises using as a base an aqueous solution of a mixture of NaOH and KOH in a molar ratio Na + :K + in the range from 70:30 to 95:5 and with a total concentration of Na + and K + in the range from 0.1 to 10 m/m % based on the total amount of the mixture.