Method and device for growing large-volume oriented monocrystals
The invention relates to a method for growing large-volume monocrystals with a uniform orientation and consisting of a melt of crystal raw material, in a device comprising a sealable housing ( 10 ) in which a melting vessel ( 20 ) with side walls ( 22 ), a bottom ( 24 ), a top opening ( 26 ) facing...
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Format: | Patent |
Sprache: | eng |
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Zusammenfassung: | The invention relates to a method for growing large-volume monocrystals with a uniform orientation and consisting of a melt of crystal raw material, in a device comprising a sealable housing (
10
) in which a melting vessel (
20
) with side walls (
22
), a bottom (
24
), a top opening (
26
) facing said bottom (
24
) and optionally a lid (
28
) are located; and at least one heating element (
50, 50
′). According to said method, a crystal raw material in the melting vessel (
20
) is heated with heating elements (
50, 50
′) to a temperature above the melting point until a melt with a surface is formed. A monocrystal is then formed on the bottom of the melting vessel by lowering the temperature to at least the crystallisation point. Said monocrystal forms a solid/liquid interphase with the melt and grows towards the melt surface on said interphase, in a direction that is perpendicular to the interphase. An even interphase with a radius of curvature of at least one metre is produced during the crystal growing process by applying a vertical, axial temperature gradient between the bottom (
24
) of the melt vessel (
20
) and its top opening (
26
) and preventing heat from entering and/or leaving through the side walls (
22
). |
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