Method and apparatus for evaporating components of multiple substance mixtures and multiple substance systems
For the evaporation of given components from initial multiple-substance mixtures and systems at subatmospheric pressure, individual portions (P 1 , P 2 , P 3 , P 4 , P 5 ) of the multiple-substance mixture and systems are placed in ring crucibles ( 17 ) stacked at several levels. Vapors of the lower...
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Sprache: | eng |
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Zusammenfassung: | For the evaporation of given components from initial multiple-substance mixtures and systems at subatmospheric pressure, individual portions (P
1
, P
2
, P
3
, P
4
, P
5
) of the multiple-substance mixture and systems are placed in ring crucibles (
17
) stacked at several levels. Vapors of the lower-boiling component are drawn off through a vapor exhaust opening in each crucible, while the top ring crucible (
17
) is closed except for its vapor exhaust opening. In order to obtain products of high purity through short diffusion path lengths and great uniformity of temperature distribution,
a) ring crucibles (
17
) are used which act as susceptors towards alternating electromagnetic fields,
b) heat bodies (
16, 21
) are arranged under and over the crucible stack, and likewise act as susceptors towards alternating electromagnetic fields,
c) the ring crucibles (
17
) and the heat bodies (
16, 21
) are heated by inductive coupling, doing so
d) with such timing that at least one of the given components of the multiple-substance mixture or system is obtained in the greatest possible purity. |
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