A Convenient and Efficient One-Pot Synthesis of 3-Acylisoxazoles Using Iron(III) Salts

A Convenient and Efficient One-Pot Synthesis of 3-Acylisoxazoles Using Iron(III) Salts

ABSTRACT 3-Acylisoxazoles were synthesized by the reaction of alkenes or alkynes with ketones (acetone or acetophenone), as both a reagent and the solvent, by three methods: iron(III) nitrate under reflux, iron(III) salt-nitrogen dioxide (NO 2 ) at room temperature, and iron(III) nitrate under micro...

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Veröffentlicht in:Synthesis (Stuttgart) 2005-12, Vol.2005 (20), p.3541-3548
Hauptverfasser: Itoh, Ken-ichi, Sakamaki, Hiroshi, Nakazato, Noriko, Horiuchi, Atsuo, Horn, Ernst, Horiuchi, C. Akira
Format: Artikel
Sprache:eng
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Zusammenfassung:ABSTRACT 3-Acylisoxazoles were synthesized by the reaction of alkenes or alkynes with ketones (acetone or acetophenone), as both a reagent and the solvent, by three methods: iron(III) nitrate under reflux, iron(III) salt-nitrogen dioxide (NO 2 ) at room temperature, and iron(III) nitrate under microwave irradiation (MW).
ISSN:0039-7881
1437-210X
DOI:10.1055/s-2005-916041