A new microcell design for use with large volume NMR tubes. Application for low natural abundance isotopes studied by NMR
A new NMR microcell design for recording the NMR spectra of low natural abundance isotopes, such as 13C, 29Si, 15N, and 17O, when sample size is limited, is described. The new cell makes sample preparation and clean up an order of magnitude easier than with a conventional microcell. Nearly 100% reco...
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| Veröffentlicht in: | Review of scientific instruments 1974-10, Vol.45 (10), p.1263-1264 |
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| Hauptverfasser: | , |
| Format: | Artikel |
| Sprache: | eng |
| Online-Zugang: | Volltext |
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| Zusammenfassung: | A new NMR microcell design for recording the NMR spectra of low natural abundance isotopes, such as 13C, 29Si, 15N, and 17O, when sample size is limited, is described. The new cell makes sample preparation and clean up an order of magnitude easier than with a conventional microcell. Nearly 100% recovery is also possible with the use of this cell design. |
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| ISSN: | 0034-6748 1089-7623 |
| DOI: | 10.1063/1.1686474 |