Stable system for multiple pulse, magic angle spinning and dynamic angle spinning NMR

A rotor‐stator system is described that is suitable for (a) homonuclear decoupling experiments on solids, and (b) dynamic angle spinning experiments. The angle of rotation can be changed by 45° in 9 ms with no loss in rotation stability when spinning at 10 kHz.

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Bibliographische Detailangaben
Veröffentlicht in:	Review of scientific instruments 1990-10, Vol.61 (10), p.2699-2701
Hauptverfasser:	Gerstein, B. C., Pan, Hong‐Jun, Pruski, M.
Format:	Artikel
Sprache:	eng
Schlagworte:	656002 - Condensed Matter Physics- General Techniques in Condensed Matter- (1987-) CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY DESIGN DYNAMIC FUNCTION STUDIES Exact sciences and technology FLUORINE 19 FLUORINE ISOTOPES Infrared, submillimeter wave, microwave and radiowave instruments, equipment and techniques Instruments, apparatus, components and techniques common to several branches of physics and astronomy ISOTOPES KEL-F LIGHT NUCLEI MEASURING INSTRUMENTS MOTION NMR SPECTRA NMR SPECTROMETERS NUCLEI ODD-EVEN NUCLEI ORGANIC CHLORINE COMPOUNDS ORGANIC COMPOUNDS ORGANIC FLUORINE COMPOUNDS ORGANIC HALOGEN COMPOUNDS ORGANIC POLYMERS Physics POLYETHYLENES POLYMERS POLYOLEFINS ROTATION SPECTRA SPECTROMETERS STABILITY STABLE ISOTOPES Submillimeter wave, microwave and radiowave spectrometers magnetic resonance spectrometers, auxiliary equipments and techniques
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Beschreibung
Zusammenfassung:	A rotor‐stator system is described that is suitable for (a) homonuclear decoupling experiments on solids, and (b) dynamic angle spinning experiments. The angle of rotation can be changed by 45° in 9 ms with no loss in rotation stability when spinning at 10 kHz.
ISSN:	0034-6748 1089-7623
DOI:	10.1063/1.1141863