Rapid synthesis of indium phosphide

A method for the high‐pressure synthesis (440 psi) of InP is investigated. Independent temperature control of a three‐zone furnace incorporating a heat pipe provides a stable temperature profile throughout the synthesis cycle. Internal/external pressure control of the quartz ampoule is maintained by...

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Veröffentlicht in:	Review of scientific instruments 1985-05, Vol.56 (5), p.716-718
Hauptverfasser:	Adamski, Joseph A., Ahern, Brian S.
Format:	Artikel
Sprache:	eng
Schlagworte:	Cross-disciplinary physics: materials science rheology Exact sciences and technology Growth from melts zone melting and refining Materials science Methods of crystal growth physics of crystal growth Physics
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Zusammenfassung:	A method for the high‐pressure synthesis (440 psi) of InP is investigated. Independent temperature control of a three‐zone furnace incorporating a heat pipe provides a stable temperature profile throughout the synthesis cycle. Internal/external pressure control of the quartz ampoule is maintained by use of a water‐cooled baffle and a temperature/pressure balancing program. Complete synthesis is achieved in less than 5 h.
ISSN:	0034-6748 1089-7623
DOI:	10.1063/1.1138212