SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINES

SOLVENT FREE OXALIC ACID CATALYZED SYNTHESIS OF 1,5-BENZODIAZEPINES

In the present study 1, 5-benzodiazepines were synthesized from a range of α, β-unsaturated ketones and o-phenylendiamine using oxalic acid 10 mol% as a catalyst under solvent free conditions. The yields of the present method are better than the reported method which explains effectiveness of oxalic...

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Veröffentlicht in:Journal of the Chilean Chemical Society 2013-12, Vol.58 (4), p.2200-2203
Hauptverfasser: SARKATE, ANIKET P, SANGSHETTI, JAIPRAKASH N, DHARBALE, NANASAHEB B, SARKATE, AJINKYA P, WAKTE, PRAVIN S, SHINDE, DEVANAND B
Format: Artikel
Sprache:eng
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CHEMISTRY, MULTIDISCIPLINARY
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Zusammenfassung:In the present study 1, 5-benzodiazepines were synthesized from a range of α, β-unsaturated ketones and o-phenylendiamine using oxalic acid 10 mol% as a catalyst under solvent free conditions. The yields of the present method are better than the reported method which explains effectiveness of oxalic acid catalyst. The cost effective, resourceful, undemanding and environment friendly are the advantageous aspects of this method.
ISSN:0717-9707
0717-9707
DOI:10.4067/S0717-97072013000400064