Rapid and safe ASAP acquisition with EXACT NMRElectronic supplementary information (ESI) available. See DOI: 10.1039/c6cc07140f

The dangerously high power levels required for fast ASAP-HSQC and ASAP-HMQC experiments are mitigated by employing EXACT NMR. The utility of this technique is demonstrated by application of the EXACT ASAP-HSQC to chemical reaction monitoring, accelerating data acquisition by up to 2 orders of magnit...

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Hauptverfasser: Ndukwe, I. E, Shchukina, A, Kazimierczuk, K, Butts, C. P
Format: Artikel
Sprache:eng
Online-Zugang:Volltext
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Zusammenfassung:The dangerously high power levels required for fast ASAP-HSQC and ASAP-HMQC experiments are mitigated by employing EXACT NMR. The utility of this technique is demonstrated by application of the EXACT ASAP-HSQC to chemical reaction monitoring, accelerating data acquisition by up to 2 orders of magnitude - providing evidence of it's value in fast quantitative NMR processes. EXACT acquisition allows the fast and safer acquisition of ASAP 2D NMR experiments in just a few seconds.
ISSN:1359-7345
1364-548X
DOI:10.1039/c6cc07140f