Efficient continuous synthesis of high purity deep eutectic solvents by twin screw extrusion

Efficient continuous synthesis of high purity deep eutectic solvents by twin screw extrusion

Mechanochemical synthesis has been applied to the rapid synthesis of Deep Eutectic Solvents (DESs), including Reline 200 (choline chloride : urea, 1 : 2), in a continuous flow methodology by Twin Screw Extrusion (TSE). This gave products in higher purity and with Space Time Yields (STYs), four order...

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Veröffentlicht in:Chemical communications (Cambridge, England) England), 2016-01, Vol.52 (22), p.4215-4218
Hauptverfasser: Crawford, D. E, Wright, L. A, James, S. L, Abbott, A. P
Format: Artikel
Sprache:eng
Schlagworte:
Chlorides
Eutectics
Extrusion
Purity
Screws
Solvents
Synthesis
Ureas
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Zusammenfassung:Mechanochemical synthesis has been applied to the rapid synthesis of Deep Eutectic Solvents (DESs), including Reline 200 (choline chloride : urea, 1 : 2), in a continuous flow methodology by Twin Screw Extrusion (TSE). This gave products in higher purity and with Space Time Yields (STYs), four orders of magnitude greater than for batch methods. Mechanochemical synthesis has been applied to the rapid synthesis of Deep Eutectic Solvents (DESs), including Reline 200 (choline chloride : urea, 1 : 2), in a continuous flow methodology by Twin Screw Extrusion (TSE).
ISSN:1359-7345
1364-548X
DOI:10.1039/c5cc09685e