Nano-silica supported acidic ionic liquid as an efficient catalyst for the multi-component synthesis of indazolophthalazine-triones and bis-indazolophthalazine-trionesElectronic supplementary information (ESI) available. See DOI: 10.1039/c3cy00344b
A supported ionic liquid bearing sulfonic acid groups was synthesized by anchoring 3-sulfopropyl-1-(3-propyltrimethoxysilane)imidazolium hydrogen sulfate onto nano-silica and characterized by FT-IR spectroscopy, elemental analysis and scanning electron microscopy (SEM) techniques. This catalyst was...
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Zusammenfassung: | A supported ionic liquid bearing sulfonic acid groups was synthesized by anchoring 3-sulfopropyl-1-(3-propyltrimethoxysilane)imidazolium hydrogen sulfate onto nano-silica and characterized by FT-IR spectroscopy, elemental analysis and scanning electron microscopy (SEM) techniques. This catalyst was used for the efficient one-pot multi-component synthesis of indazolophthalazine-triones and bis-indazolophthalazine-triones. Moreover, the catalyst could be reused at least seven times without any significant loss of activity.
A supported ionic liquid bearing sulfonic acid groups was applied as a reusable catalyst for a one-pot multi-component synthesis of indazolophthalazine-triones derivatives. |
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ISSN: | 2044-4753 2044-4761 |
DOI: | 10.1039/c3cy00344b |