Silica sulfuric acid coated on SnFe2O4 MNPs: synthesis, characterization and catalytic applications in the synthesis of polyhydroquinolines

An efficient and heterogeneous novel magnetic solid sulfuric acid, immobilized on silica functionalized SnFe2O4, was successfully synthesized, characterized, and employed as a novel recoverable nanocatalyst for the synthesis of biologically active polyhydroquinoline derivatives. The SnFe2O4@SiO2–SO3...

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Veröffentlicht in:RSC advances 2022-05, Vol.12 (23), p.14397-14410
Hauptverfasser: Esmaili, Soheila, Khazaei, Ardeshir, Ghorbani-Choghamarani, Arash, Mohammadi, Masoud
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Sprache:eng
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Zusammenfassung:An efficient and heterogeneous novel magnetic solid sulfuric acid, immobilized on silica functionalized SnFe2O4, was successfully synthesized, characterized, and employed as a novel recoverable nanocatalyst for the synthesis of biologically active polyhydroquinoline derivatives. The SnFe2O4@SiO2–SO3H was easily synthesized and confirmed using various spectroscopic techniques, including FT-IR, XRD, EDX, Map, TGA, SEM and TEM analyses. The catalytic behavior of the resulting catalyst system was investigated in the Hantzsch synthesis of polyhydroquinoline derivatives. The desired products were obtained with high conversions and excellent reusability.
ISSN:2046-2069
DOI:10.1039/d2ra01202b