Flow Synthesis of Diaryliodonium Triflates
A safe and scalable synthesis of diaryliodonium triflates was achieved using a practical continuous-flow design. A wide array of electron-rich to electron-deficient arenes could readily be transformed to their respective diaryliodonium salts on a gram scale, with residence times varying from 2 to 60...
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| Veröffentlicht in: | Journal of organic chemistry 2017-11, Vol.82 (22), p.11735-11741 |
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| Hauptverfasser: | , , , |
| Format: | Artikel |
| Sprache: | eng |
| Online-Zugang: | Volltext |
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| Zusammenfassung: | A safe and scalable synthesis of diaryliodonium triflates was achieved using a practical continuous-flow design. A wide array of electron-rich to electron-deficient arenes could readily be transformed to their respective diaryliodonium salts on a gram scale, with residence times varying from 2 to 60 s (44 examples). |
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| ISSN: | 0022-3263 1520-6904 |
| DOI: | 10.1021/acs.joc.7b01346 |