Crystal structure of 3-amino-pyridinium 1'-carb-oxy-ferrocene-1-carboxyl-ate
The structure of the title salt, (C H N )[Fe(C H O )(C H O )], consists of 3-amino-pyridinium cations and 1'-carb-oxy-ferrocene-1-carboxyl-ate monoanions. The ferrocenyl moiety of the anion adopts a typical sandwich structure, with Fe-C distances in the range 2.0270 (15)-2.0568 (17) Å. The anio...
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| Veröffentlicht in: | Acta crystallographica. Section E, Crystallographic communications Crystallographic communications, 2017-06, Vol.73 (Pt 6), p.856-858 |
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| container_issue | Pt 6 |
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| container_title | Acta crystallographica. Section E, Crystallographic communications |
| container_volume | 73 |
| creator | Medved'ko, Aleksei V Churakov, Andrei V Yu, Haojie Li, Wang Vatsadze, Sergey Z |
| description | The structure of the title salt, (C
H
N
)[Fe(C
H
O
)(C
H
O
)], consists of 3-amino-pyridinium cations and 1'-carb-oxy-ferrocene-1-carboxyl-ate monoanions. The ferrocenyl moiety of the anion adopts a typical sandwich structure, with Fe-C distances in the range 2.0270 (15)-2.0568 (17) Å. The anion possesses an eclipsed conformation, with the torsion angle φ (C
-Cp
-Cp
- C
) equal to 66.0°. The conformations of other 1'-carb-oxy-ferrocene-1-carboxyl-ate monoanions are compared and analyzed on the basis of literature data. |
| doi_str_mv | 10.1107/S2056989017007058 |
| format | Article |
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H
N
)[Fe(C
H
O
)(C
H
O
)], consists of 3-amino-pyridinium cations and 1'-carb-oxy-ferrocene-1-carboxyl-ate monoanions. The ferrocenyl moiety of the anion adopts a typical sandwich structure, with Fe-C distances in the range 2.0270 (15)-2.0568 (17) Å. The anion possesses an eclipsed conformation, with the torsion angle φ (C
-Cp
-Cp
- C
) equal to 66.0°. The conformations of other 1'-carb-oxy-ferrocene-1-carboxyl-ate monoanions are compared and analyzed on the basis of literature data.</description><identifier>ISSN: 2056-9890</identifier><identifier>EISSN: 2056-9890</identifier><identifier>DOI: 10.1107/S2056989017007058</identifier><identifier>PMID: 28638644</identifier><language>eng</language><publisher>England: International Union of Crystallography</publisher><subject>Research Communications</subject><ispartof>Acta crystallographica. Section E, Crystallographic communications, 2017-06, Vol.73 (Pt 6), p.856-858</ispartof><rights>Medved'ko et al. 2017 2017</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><orcidid>0000-0003-3336-4022 ; 0000-0001-7884-8579</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC5458309/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC5458309/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,315,729,782,786,866,887,27931,27932,53798,53800</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/28638644$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Medved'ko, Aleksei V</creatorcontrib><creatorcontrib>Churakov, Andrei V</creatorcontrib><creatorcontrib>Yu, Haojie</creatorcontrib><creatorcontrib>Li, Wang</creatorcontrib><creatorcontrib>Vatsadze, Sergey Z</creatorcontrib><title>Crystal structure of 3-amino-pyridinium 1'-carb-oxy-ferrocene-1-carboxyl-ate</title><title>Acta crystallographica. Section E, Crystallographic communications</title><addtitle>Acta Crystallogr E Crystallogr Commun</addtitle><description>The structure of the title salt, (C
H
N
)[Fe(C
H
O
)(C
H
O
)], consists of 3-amino-pyridinium cations and 1'-carb-oxy-ferrocene-1-carboxyl-ate monoanions. The ferrocenyl moiety of the anion adopts a typical sandwich structure, with Fe-C distances in the range 2.0270 (15)-2.0568 (17) Å. The anion possesses an eclipsed conformation, with the torsion angle φ (C
-Cp
-Cp
- C
) equal to 66.0°. The conformations of other 1'-carb-oxy-ferrocene-1-carboxyl-ate monoanions are compared and analyzed on the basis of literature data.</description><subject>Research Communications</subject><issn>2056-9890</issn><issn>2056-9890</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNpVkE1LxDAQhoMo7rLuD_AiveklmslH21wEWfyCBQ_quaRpopG2qUkr9t_b1VXW0wzPDO_7ziB0DOQcgGQXj5SIVOaSQEZIRkS-h-YbhDdsf6efoWWMb4QQ4IKlgh6iGc1Tlqecz9F6FcbYqzqJfRh0PwSTeJswrBrXetyNwVWudUOTwCnWKpTYf47YmhC8Nq3B8A0nVmPVmyN0YFUdzXJbF-j55vppdYfXD7f3q6s17gBAYmoIlxIkVBk1huncaKaJVVVWWiGtkrnhwtqUmYrrTGrGQE9X6hIIJ5QAW6DLH91uKBtTTUn6oOqiC65RYSy8csX_Seteixf_UQguckbkJHC2FQj-fTCxLxoXtalr1Ro_xGLKRlPgFLJp9WTX68_k94XsC7d6dOI</recordid><startdate>20170601</startdate><enddate>20170601</enddate><creator>Medved'ko, Aleksei V</creator><creator>Churakov, Andrei V</creator><creator>Yu, Haojie</creator><creator>Li, Wang</creator><creator>Vatsadze, Sergey Z</creator><general>International Union of Crystallography</general><scope>NPM</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0003-3336-4022</orcidid><orcidid>https://orcid.org/0000-0001-7884-8579</orcidid></search><sort><creationdate>20170601</creationdate><title>Crystal structure of 3-amino-pyridinium 1'-carb-oxy-ferrocene-1-carboxyl-ate</title><author>Medved'ko, Aleksei V ; Churakov, Andrei V ; Yu, Haojie ; Li, Wang ; Vatsadze, Sergey Z</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p1119-2e0499191d72ee3c8ec3c0fad7bf59fa98e45ff63ed4c79c331c017cb10402013</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Research Communications</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Medved'ko, Aleksei V</creatorcontrib><creatorcontrib>Churakov, Andrei V</creatorcontrib><creatorcontrib>Yu, Haojie</creatorcontrib><creatorcontrib>Li, Wang</creatorcontrib><creatorcontrib>Vatsadze, Sergey Z</creatorcontrib><collection>PubMed</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Acta crystallographica. Section E, Crystallographic communications</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Medved'ko, Aleksei V</au><au>Churakov, Andrei V</au><au>Yu, Haojie</au><au>Li, Wang</au><au>Vatsadze, Sergey Z</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Crystal structure of 3-amino-pyridinium 1'-carb-oxy-ferrocene-1-carboxyl-ate</atitle><jtitle>Acta crystallographica. Section E, Crystallographic communications</jtitle><addtitle>Acta Crystallogr E Crystallogr Commun</addtitle><date>2017-06-01</date><risdate>2017</risdate><volume>73</volume><issue>Pt 6</issue><spage>856</spage><epage>858</epage><pages>856-858</pages><issn>2056-9890</issn><eissn>2056-9890</eissn><abstract>The structure of the title salt, (C
H
N
)[Fe(C
H
O
)(C
H
O
)], consists of 3-amino-pyridinium cations and 1'-carb-oxy-ferrocene-1-carboxyl-ate monoanions. The ferrocenyl moiety of the anion adopts a typical sandwich structure, with Fe-C distances in the range 2.0270 (15)-2.0568 (17) Å. The anion possesses an eclipsed conformation, with the torsion angle φ (C
-Cp
-Cp
- C
) equal to 66.0°. The conformations of other 1'-carb-oxy-ferrocene-1-carboxyl-ate monoanions are compared and analyzed on the basis of literature data.</abstract><cop>England</cop><pub>International Union of Crystallography</pub><pmid>28638644</pmid><doi>10.1107/S2056989017007058</doi><tpages>3</tpages><orcidid>https://orcid.org/0000-0003-3336-4022</orcidid><orcidid>https://orcid.org/0000-0001-7884-8579</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | Research Communications |
| title | Crystal structure of 3-amino-pyridinium 1'-carb-oxy-ferrocene-1-carboxyl-ate |
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