1020 MHz single-channel proton fast magic angle spinning solid-state NMR spectroscopy

This study reports a first successful demonstration of a single channel proton 3D and 2D high-throughput ultrafast magic angle spinning (MAS) solid-state NMR techniques in an ultra-high magnetic field (1020 MHz) NMR spectrometer comprised of HTS/LTS magnet. High spectral resolution is well demonstra...

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Veröffentlicht in:Journal of magnetic resonance (1997) 2015-12, Vol.261, p.1-5
Hauptverfasser: Pandey, Manoj Kumar, Zhang, Rongchun, Hashi, Kenjiro, Ohki, Shinobu, Nishijima, Gen, Matsumoto, Shinji, Noguchi, Takashi, Deguchi, Kenzo, Goto, Atsushi, Shimizu, Tadashi, Maeda, Hideaki, Takahashi, Masato, Yanagisawa, Yoshinori, Yamazaki, Toshio, Iguchi, Seiya, Tanaka, Ryoji, Nemoto, Takahiro, Miyamoto, Tetsuo, Suematsu, Hiroto, Saito, Kazuyoshi, Miki, Takashi, Ramamoorthy, Ayyalusamy, Nishiyama, Yusuke
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Sprache:eng
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Zusammenfassung:This study reports a first successful demonstration of a single channel proton 3D and 2D high-throughput ultrafast magic angle spinning (MAS) solid-state NMR techniques in an ultra-high magnetic field (1020 MHz) NMR spectrometer comprised of HTS/LTS magnet. High spectral resolution is well demonstrated.
ISSN:1090-7807
1096-0856
DOI:10.1016/j.jmr.2015.10.003