Enhanced electrical properties in sub-10-nm WO3 nanoflakes prepared via a two-step sol-gel-exfoliation method
The morphology and electrical properties of orthorhombic β-WO 3 nanoflakes with thickness of ~7 to 9 nm were investigated at the nanoscale with a combination of scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), current sensing force spectroscopy atomic force microscopy...
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| Veröffentlicht in: | Nanoscale research letters 2014-08, Vol.9 (1), p.401-401, Article 401 |
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| container_title | Nanoscale research letters |
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| creator | Zhuiykov, Serge Kats, Eugene |
| description | The morphology and electrical properties of orthorhombic β-WO
3
nanoflakes with thickness of ~7 to 9 nm were investigated at the nanoscale with a combination of scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), current sensing force spectroscopy atomic force microscopy (CSFS-AFM, or PeakForce TUNA™), Fourier transform infra-red absorption spectroscopy (FTIR), linear sweep voltammetry (LSV) and Raman spectroscopy techniques. CSFS-AFM analysis established good correlation between the topography of the developed nanostructures and various features of WO
3
nanoflakes synthesized via a two-step sol-gel-exfoliation method. It was determined that β-WO
3
nanoflakes annealed at 550°C possess distinguished and exceptional thickness-dependent properties in comparison with the bulk, micro and nanostructured WO
3
synthesized at alternative temperatures. |
| doi_str_mv | 10.1186/1556-276X-9-401 |
| format | Article |
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3
nanoflakes with thickness of ~7 to 9 nm were investigated at the nanoscale with a combination of scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), current sensing force spectroscopy atomic force microscopy (CSFS-AFM, or PeakForce TUNA™), Fourier transform infra-red absorption spectroscopy (FTIR), linear sweep voltammetry (LSV) and Raman spectroscopy techniques. CSFS-AFM analysis established good correlation between the topography of the developed nanostructures and various features of WO
3
nanoflakes synthesized via a two-step sol-gel-exfoliation method. It was determined that β-WO
3
nanoflakes annealed at 550°C possess distinguished and exceptional thickness-dependent properties in comparison with the bulk, micro and nanostructured WO
3
synthesized at alternative temperatures.</description><identifier>ISSN: 1931-7573</identifier><identifier>ISSN: 1556-276X</identifier><identifier>EISSN: 1556-276X</identifier><identifier>DOI: 10.1186/1556-276X-9-401</identifier><identifier>PMID: 25221453</identifier><language>eng</language><publisher>New York: Springer New York</publisher><subject>Chemistry and Materials Science ; Materials Science ; Molecular Medicine ; Nano Express ; Nanochemistry ; Nanoscale Science and Technology ; Nanotechnology ; Nanotechnology and Microengineering</subject><ispartof>Nanoscale research letters, 2014-08, Vol.9 (1), p.401-401, Article 401</ispartof><rights>Zhuiykov and Kats; licensee Springer. 2014. This article is published under license to BioMed Central Ltd. This is an Open Access article distributed under the terms of the Creative Commons Attribution License ( ), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly credited.</rights><rights>Copyright © 2014 Zhuiykov and Kats; licensee Springer. 2014 Zhuiykov and Kats; licensee Springer.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c500t-6c03f7593f8eb8d13d9c4dc41a20030449e187f7d88ec2e77a98959813f1efc83</citedby><cites>FETCH-LOGICAL-c500t-6c03f7593f8eb8d13d9c4dc41a20030449e187f7d88ec2e77a98959813f1efc83</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC4150682/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC4150682/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,864,885,27923,27924,53790,53792</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/25221453$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Zhuiykov, Serge</creatorcontrib><creatorcontrib>Kats, Eugene</creatorcontrib><title>Enhanced electrical properties in sub-10-nm WO3 nanoflakes prepared via a two-step sol-gel-exfoliation method</title><title>Nanoscale research letters</title><addtitle>Nanoscale Res Lett</addtitle><addtitle>Nanoscale Res Lett</addtitle><description>The morphology and electrical properties of orthorhombic β-WO
3
nanoflakes with thickness of ~7 to 9 nm were investigated at the nanoscale with a combination of scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), current sensing force spectroscopy atomic force microscopy (CSFS-AFM, or PeakForce TUNA™), Fourier transform infra-red absorption spectroscopy (FTIR), linear sweep voltammetry (LSV) and Raman spectroscopy techniques. CSFS-AFM analysis established good correlation between the topography of the developed nanostructures and various features of WO
3
nanoflakes synthesized via a two-step sol-gel-exfoliation method. It was determined that β-WO
3
nanoflakes annealed at 550°C possess distinguished and exceptional thickness-dependent properties in comparison with the bulk, micro and nanostructured WO
3
synthesized at alternative temperatures.</description><subject>Chemistry and Materials Science</subject><subject>Materials Science</subject><subject>Molecular Medicine</subject><subject>Nano Express</subject><subject>Nanochemistry</subject><subject>Nanoscale Science and Technology</subject><subject>Nanotechnology</subject><subject>Nanotechnology and Microengineering</subject><issn>1931-7573</issn><issn>1556-276X</issn><issn>1556-276X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><sourceid>C6C</sourceid><recordid>eNp1kM9LHDEUx0OpVGt77k3yD6Qmk8kkuQhl0VYQvFT0FrKZl93YmWRIZlf735tl66KHnt7jfX88-CD0jdHvjKnunAnRkUZ2D0STlrIP6ORw-Vh3zRmRQvJj9LmUR0pbSWX3CR03omlYK_gJGi_j2kYHPYYB3JyDswOecpogzwEKDhGXzZIwSuKI7285jjYmP9g_VZsyTDbX6DZYbPH8lEiZYcIlDWQFA4Fnn4Zg55AiHmFep_4LOvJ2KPD13zxFd1eXvxe_yM3tz-vFjxviBKUz6RzlXgrNvYKl6hnvtWt71zLbUMpp22pgSnrZKwWuASmtVlpoxbhn4J3ip-hi3zttliP0DuKc7WCmHEab_5pkg3mvxLA2q7Q1LRO0U00tON8XuJxKyeAPWUbNjrzZcTY7zkabSr4mzt6-PPhfUVcD3RtKleIKsnlMmxwrhv92vgAwsI__</recordid><startdate>20140818</startdate><enddate>20140818</enddate><creator>Zhuiykov, Serge</creator><creator>Kats, Eugene</creator><general>Springer New York</general><general>Springer</general><scope>C6C</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>5PM</scope></search><sort><creationdate>20140818</creationdate><title>Enhanced electrical properties in sub-10-nm WO3 nanoflakes prepared via a two-step sol-gel-exfoliation method</title><author>Zhuiykov, Serge ; Kats, Eugene</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c500t-6c03f7593f8eb8d13d9c4dc41a20030449e187f7d88ec2e77a98959813f1efc83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Chemistry and Materials Science</topic><topic>Materials Science</topic><topic>Molecular Medicine</topic><topic>Nano Express</topic><topic>Nanochemistry</topic><topic>Nanoscale Science and Technology</topic><topic>Nanotechnology</topic><topic>Nanotechnology and Microengineering</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhuiykov, Serge</creatorcontrib><creatorcontrib>Kats, Eugene</creatorcontrib><collection>Springer Nature OA Free Journals</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Nanoscale research letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhuiykov, Serge</au><au>Kats, Eugene</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Enhanced electrical properties in sub-10-nm WO3 nanoflakes prepared via a two-step sol-gel-exfoliation method</atitle><jtitle>Nanoscale research letters</jtitle><stitle>Nanoscale Res Lett</stitle><addtitle>Nanoscale Res Lett</addtitle><date>2014-08-18</date><risdate>2014</risdate><volume>9</volume><issue>1</issue><spage>401</spage><epage>401</epage><pages>401-401</pages><artnum>401</artnum><issn>1931-7573</issn><issn>1556-276X</issn><eissn>1556-276X</eissn><abstract>The morphology and electrical properties of orthorhombic β-WO
3
nanoflakes with thickness of ~7 to 9 nm were investigated at the nanoscale with a combination of scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX), current sensing force spectroscopy atomic force microscopy (CSFS-AFM, or PeakForce TUNA™), Fourier transform infra-red absorption spectroscopy (FTIR), linear sweep voltammetry (LSV) and Raman spectroscopy techniques. CSFS-AFM analysis established good correlation between the topography of the developed nanostructures and various features of WO
3
nanoflakes synthesized via a two-step sol-gel-exfoliation method. It was determined that β-WO
3
nanoflakes annealed at 550°C possess distinguished and exceptional thickness-dependent properties in comparison with the bulk, micro and nanostructured WO
3
synthesized at alternative temperatures.</abstract><cop>New York</cop><pub>Springer New York</pub><pmid>25221453</pmid><doi>10.1186/1556-276X-9-401</doi><tpages>1</tpages><oa>free_for_read</oa></addata></record> |
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| issn | 1931-7573 1556-276X 1556-276X |
| language | eng |
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| source | DOAJ Directory of Open Access Journals; PubMed Central Open Access; EZB-FREE-00999 freely available EZB journals; PubMed Central; Free Full-Text Journals in Chemistry |
| subjects | Chemistry and Materials Science Materials Science Molecular Medicine Nano Express Nanochemistry Nanoscale Science and Technology Nanotechnology Nanotechnology and Microengineering |
| title | Enhanced electrical properties in sub-10-nm WO3 nanoflakes prepared via a two-step sol-gel-exfoliation method |
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