Cytenamide-butyric acid (1/1)

Cytenamide-butyric acid (1/1)

Cytenamide forms a 1:1 solvate with butyric acid [systematic name: 5H-dibenzo[a,d]cyclo-hepta-triene-5-carboxamide-butanoic acid (1/1)], C(16)H(13)NO·C(4)H(8)O(2). The title compound crystallizes with one mol-ecule of cytenamide and one of butyric acid in the asymmetric unit; these mol-ecules are li...

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Veröffentlicht in:Acta crystallographica. Section E, Structure reports online Structure reports online, 2008-06, Vol.64 (Pt 7), p.o1295-o1296
Hauptverfasser: Johnston, Andrea, Florence, Alastair J, Fabbiani, Francesca J A, Shankland, Kenneth, Bedford, Colin T
Format: Artikel
Sprache:eng
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Organic Papers
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Zusammenfassung:Cytenamide forms a 1:1 solvate with butyric acid [systematic name: 5H-dibenzo[a,d]cyclo-hepta-triene-5-carboxamide-butanoic acid (1/1)], C(16)H(13)NO·C(4)H(8)O(2). The title compound crystallizes with one mol-ecule of cytenamide and one of butyric acid in the asymmetric unit; these mol-ecules are linked by N-H⋯O and O-H⋯O hydrogen bonds to form an R(2) (2)(8) heterodimer motif. Pairs of adjacent motifs are further connected via N-H⋯O inter-actions to form a discrete centrosymmetric assembly.
ISSN:1600-5368
1600-5368
DOI:10.1107/S1600536808018059