Sb(iii)/Gum Arabic composite as a new natural-based environmentally green catalyst for the one-pot pseudo-four-component synthesis of 2H-indazolo[2,1-b] phthalazinetriones

Sb(iii)–Gum Arabic composite as a unique natural-based and nontoxic catalyst was synthesized and characterized by FT-IR, XRD, TGA, ICP, BET, EDX and mapping. A four-component reaction of phthalic anhydride, hydrazinium hydroxide, aldehyde, and dimedone has been carried out in the presence of Sb(iii)...

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Veröffentlicht in:RSC advances 2023-06, Vol.13 (26), p.17869-17873
Hauptverfasser: Keihanfar, Mina, Bi Bi Fatemeh Mirjalili, Bamoniri, Abdolhamid
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Sprache:eng
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Zusammenfassung:Sb(iii)–Gum Arabic composite as a unique natural-based and nontoxic catalyst was synthesized and characterized by FT-IR, XRD, TGA, ICP, BET, EDX and mapping. A four-component reaction of phthalic anhydride, hydrazinium hydroxide, aldehyde, and dimedone has been carried out in the presence of Sb(iii)/Gum Arabic composite to synthesise 2H-indazolo[2,1-b] phthalazine triones. The advantages of the present protocol are the appropriate reaction times, eco-friendly nature and high yields.
ISSN:2046-2069
DOI:10.1039/d3ra02556j