Determination of glycarbylamide residues in chicken tissues by HPLC with post-column reaction

A newly developed HPLC method for determination of glycarbylamide (GB) in chicken liver was applied to other tissues (muscle, fat and kidney). The recoveries of GB in muscle, fat and kidney were 87.2% (CV 0.5), 91.3% (CV 4.7), 79.7% (CV 1.0), respectively. The detection limit of GB was 0.01 ppm. GB...

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Veröffentlicht in:	Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) 2006/12/25, Vol.47(6), pp.293-296
Hauptverfasser:	Mizuno, Y.(Japan. Ministry of Agriculture, Forestry and Fisheries, Kokubunji, Tokyo. National Veterinary Assay Lab.), Horiuchi, T, Sekiya, T, Tajima, N, Maeda, M, Hamamoto, K
Format:	Artikel
Sprache:	jpn
Schlagworte:	Adipose Tissue - metabolism ANALYTICAL METHODS Animals chicken CHICKENS Chromatography, High Pressure Liquid - methods Coccidiostats - administration & dosage Coccidiostats - analysis Drug Residues - analysis DRUGS Female Food Analysis - methods glycarbylamide HPLC Imidazoles - administration & dosage Imidazoles - analysis Kidney - metabolism Liver - metabolism Male Meat - analysis MEDICAMENT MEDICAMENTOS Muscles - metabolism POLLO post-column reaction POULET RESIDU residue RESIDUES RESIDUOS TECHNIQUE ANALYTIQUE TECNICAS ANALITICAS Time Factors Tissue Distribution
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Zusammenfassung:	A newly developed HPLC method for determination of glycarbylamide (GB) in chicken liver was applied to other tissues (muscle, fat and kidney). The recoveries of GB in muscle, fat and kidney were 87.2% (CV 0.5), 91.3% (CV 4.7), 79.7% (CV 1.0), respectively. The detection limit of GB was 0.01 ppm. GB concentrations were determined by this method in tissues (muscle, fat, liver and kidney) from chickens sacrificed 5 days after oral administration of GB mixed in feed at 60 mg/kg of feed for 7 days. GB was not detected in these chicken tissues.
ISSN:	0015-6426 1882-1006
DOI:	10.3358/shokueishi.47.293