Synthesis of novel pompon-like porous SnO₂ and its application in lithium-ion battery

Novel pompon-like porous SnO₂ with an average diameter of 900nm has been successfully synthesized via a simple hydrothermal process with subsequent calcination treatment at 600°C for 2h in air. The crystalline structure and morphology of the resulting product were characterized by X-ray diffraction,...

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Veröffentlicht in:Materials letters 2012, Vol.66 (1), p.193-195
Hauptverfasser: Sun, Xiaolei, Wang, Xinghui, Qin, Yanli, Li, Xiuwan, Qiao, Li, Feng, Na, Hu, Duokai, He, Deyan
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Sprache:eng
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Zusammenfassung:Novel pompon-like porous SnO₂ with an average diameter of 900nm has been successfully synthesized via a simple hydrothermal process with subsequent calcination treatment at 600°C for 2h in air. The crystalline structure and morphology of the resulting product were characterized by X-ray diffraction, micro-Raman spectrometer, field-emission scanning electron microscopy and transmission electron microscopy. The results indicate that the product is composed of self-assembly SnO₂ pompon with a high purity tetragonal rutile-like structure. The lithium storage property of the obtained pompon-like porous SnO₂ was evaluated by conventional discharge/charge test, showing a high initial discharge capacity of 1895 mAh g⁻¹ at a current density of 100mAg⁻¹.
ISSN:0167-577X
1873-4979
DOI:10.1016/j.matlet.2011.08.084