Single step synthesis of SnO sub(2)-SiO sub(2) core-shell microcables

Silica sheathed SnO sub(2) microcables were grown directly on a Si substrate via a simple one-step vapor phase method, with high yield and uniform distribution, using gold as a catalyst. The morphology, the microstructure and the chemical composition of the microcables were characterized by means of...

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Veröffentlicht in:Journal of crystal growth 2011-09, Vol.330 (1), p.22-29
Hauptverfasser: Filippo, Emanuela, Manno, Daniela, De Bartolomeo, AR, Serra, Antonio
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Sprache:eng
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Zusammenfassung:Silica sheathed SnO sub(2) microcables were grown directly on a Si substrate via a simple one-step vapor phase method, with high yield and uniform distribution, using gold as a catalyst. The morphology, the microstructure and the chemical composition of the microcables were characterized by means of scanning electron microscopy coupled with an X-ray microanalysis equipment, transmission electron microscopy, selected area diffraction pattern, X-ray diffraction and UV-vis and Raman spectroscopies. A possible growth mechanism of the microcables was also proposed on the basis of study of the products obtained at different thermal treatment times in the furnace.
ISSN:0022-0248
DOI:10.1016/j.jcrysgro.2011.06.045