Fabrication and electrical properties of barium strontium titanate thick films by modified sol–gel method
A modified sol–gel method has been developed to prepare for the barium strontium titanate (Ba 0.6 Sr 0.4 TiO 3 , BST) thick films. The films were deposited on either Pd–Ag electroded alumina substrates (Pd–Ag/Al 2 O 3 ) or silver electroded alumina (Ag/Al 2 O 3 ) substrates by spin coating technique...
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Veröffentlicht in: | Journal of electroceramics 2008-12, Vol.21 (1-4), p.503-507 |
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creator | Zhang, Hongfang Zhang, Liangying Yao, Xi |
description | A modified sol–gel method has been developed to prepare for the barium strontium titanate (Ba
0.6
Sr
0.4
TiO
3
, BST) thick films. The films were deposited on either Pd–Ag electroded alumina substrates (Pd–Ag/Al
2
O
3
) or silver electroded alumina (Ag/Al
2
O
3
) substrates by spin coating technique or screen printing technique. The thickness of the film was in the range of 2–10 μm. The key point of the process is to disperse fine-grained BST ceramic powders prepared by high energy ball mill into BST sol solution to form a slurry for spin coating and screen printing. In order to enhance the stability of the slurry and to avoid crack formation of the thick film, organic macromolecular poly-vinylpyrrolidone (PVP) was added to the sol solution. The structure and surface morphology of the films were studied by X-ray diffraction and Scanning Electron Microscope (SEM) techniques. It is revealed that the thick films exhibit pure perovskite phase and are crack-free, dense and homogeneous. The dielectric constant and loss tangent of the thick films are about 1200 and 0.01, at 10 °C and 1 KHz, respectively. |
doi_str_mv | 10.1007/s10832-007-9229-9 |
format | Article |
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0.6
Sr
0.4
TiO
3
, BST) thick films. The films were deposited on either Pd–Ag electroded alumina substrates (Pd–Ag/Al
2
O
3
) or silver electroded alumina (Ag/Al
2
O
3
) substrates by spin coating technique or screen printing technique. The thickness of the film was in the range of 2–10 μm. The key point of the process is to disperse fine-grained BST ceramic powders prepared by high energy ball mill into BST sol solution to form a slurry for spin coating and screen printing. In order to enhance the stability of the slurry and to avoid crack formation of the thick film, organic macromolecular poly-vinylpyrrolidone (PVP) was added to the sol solution. The structure and surface morphology of the films were studied by X-ray diffraction and Scanning Electron Microscope (SEM) techniques. It is revealed that the thick films exhibit pure perovskite phase and are crack-free, dense and homogeneous. The dielectric constant and loss tangent of the thick films are about 1200 and 0.01, at 10 °C and 1 KHz, respectively.</description><identifier>ISSN: 1385-3449</identifier><identifier>EISSN: 1573-8663</identifier><identifier>DOI: 10.1007/s10832-007-9229-9</identifier><identifier>CODEN: JOELFJ</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Aluminum oxide ; Applied sciences ; Barium strontium titanates ; Building materials. Ceramics. Glasses ; Ceramic industries ; Ceramics ; Characterization and Evaluation of Materials ; Chemical industry and chemicals ; Chemistry and Materials Science ; Composites ; Cross-disciplinary physics: materials science; rheology ; Crystallography and Scattering Methods ; Electrochemistry ; Electrotechnical and electronic ceramics ; Exact sciences and technology ; Glass ; Liquid phase epitaxy; deposition from liquid phases (melts, solutions, and surface layers on liquids) ; Materials Science ; Methods of deposition of films and coatings; film growth and epitaxy ; Natural Materials ; Optical and Electronic Materials ; Palladium ; Physics ; Scanning electron microscopy ; Screen printing ; Silver ; Sol gel process ; Spin coating ; Technical ceramics ; Thick films</subject><ispartof>Journal of electroceramics, 2008-12, Vol.21 (1-4), p.503-507</ispartof><rights>Springer Science+Business Media, LLC 2007</rights><rights>2009 INIST-CNRS</rights><rights>Springer Science+Business Media, LLC 2008</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c408t-3748f04dd0cd8e74263d7b28785dca96729f9f4fff94d81115ec49789b1205e63</citedby><cites>FETCH-LOGICAL-c408t-3748f04dd0cd8e74263d7b28785dca96729f9f4fff94d81115ec49789b1205e63</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10832-007-9229-9$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10832-007-9229-9$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>309,310,314,777,781,786,787,23911,23912,25121,27905,27906,41469,42538,51300</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=21061937$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Zhang, Hongfang</creatorcontrib><creatorcontrib>Zhang, Liangying</creatorcontrib><creatorcontrib>Yao, Xi</creatorcontrib><title>Fabrication and electrical properties of barium strontium titanate thick films by modified sol–gel method</title><title>Journal of electroceramics</title><addtitle>J Electroceram</addtitle><description>A modified sol–gel method has been developed to prepare for the barium strontium titanate (Ba
0.6
Sr
0.4
TiO
3
, BST) thick films. The films were deposited on either Pd–Ag electroded alumina substrates (Pd–Ag/Al
2
O
3
) or silver electroded alumina (Ag/Al
2
O
3
) substrates by spin coating technique or screen printing technique. The thickness of the film was in the range of 2–10 μm. The key point of the process is to disperse fine-grained BST ceramic powders prepared by high energy ball mill into BST sol solution to form a slurry for spin coating and screen printing. In order to enhance the stability of the slurry and to avoid crack formation of the thick film, organic macromolecular poly-vinylpyrrolidone (PVP) was added to the sol solution. The structure and surface morphology of the films were studied by X-ray diffraction and Scanning Electron Microscope (SEM) techniques. It is revealed that the thick films exhibit pure perovskite phase and are crack-free, dense and homogeneous. The dielectric constant and loss tangent of the thick films are about 1200 and 0.01, at 10 °C and 1 KHz, respectively.</description><subject>Aluminum oxide</subject><subject>Applied sciences</subject><subject>Barium strontium titanates</subject><subject>Building materials. Ceramics. Glasses</subject><subject>Ceramic industries</subject><subject>Ceramics</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical industry and chemicals</subject><subject>Chemistry and Materials Science</subject><subject>Composites</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Crystallography and Scattering Methods</subject><subject>Electrochemistry</subject><subject>Electrotechnical and electronic ceramics</subject><subject>Exact sciences and technology</subject><subject>Glass</subject><subject>Liquid phase epitaxy; deposition from liquid phases (melts, solutions, and surface layers on liquids)</subject><subject>Materials Science</subject><subject>Methods of deposition of films and coatings; film growth and epitaxy</subject><subject>Natural Materials</subject><subject>Optical and Electronic Materials</subject><subject>Palladium</subject><subject>Physics</subject><subject>Scanning electron microscopy</subject><subject>Screen printing</subject><subject>Silver</subject><subject>Sol gel process</subject><subject>Spin coating</subject><subject>Technical ceramics</subject><subject>Thick films</subject><issn>1385-3449</issn><issn>1573-8663</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2008</creationdate><recordtype>article</recordtype><recordid>eNp9kc1KHjEUhoeiUP8uoLtQUFfT5neSLItUWxDc1HXIJCcanZl8TfIt3PUeeodeSTN8UqFQV-fl5Dkv5-Ttug8EfyIYy8-FYMVo32SvKdW9ftcdECFZr4aB7TXNlOgZ5_p9d1jKA8ZYK04OusdLO-bobI1pQXbxCCZwde1MaJPTBnKNUFAKaLQ5bmdUak5LXVWN1S62Aqr30T2iEKe5oPEJzcnHEMGjkqbnX7_vYEIz1Pvkj7v9YKcCJy_1qLu9_Prj4lt_fXP1_eLLde84VrVnkquAuffYeQWS04F5OVIllfDO6kFSHXTgIQTNvSKECHBcS6VHQrGAgR115zvfdsDPLZRq5lgcTJNdIG2L0YQPAgvMGnn2JsmEUpyJ1fLjP-BD2ualXWGUIgPTjK8Q2UEup1IyBLPJcbb5yRBs1pTMLiWzyjUlo9vM6YuxLe3PQ7aLi-XvICV4IJrJxtEdV9rTcgf5dYH_m_8BE9ajIg</recordid><startdate>20081201</startdate><enddate>20081201</enddate><creator>Zhang, Hongfang</creator><creator>Zhang, Liangying</creator><creator>Yao, Xi</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SP</scope><scope>7SR</scope><scope>7U5</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>7QF</scope></search><sort><creationdate>20081201</creationdate><title>Fabrication and electrical properties of barium strontium titanate thick films by modified sol–gel method</title><author>Zhang, Hongfang ; Zhang, Liangying ; Yao, Xi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c408t-3748f04dd0cd8e74263d7b28785dca96729f9f4fff94d81115ec49789b1205e63</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2008</creationdate><topic>Aluminum oxide</topic><topic>Applied sciences</topic><topic>Barium strontium titanates</topic><topic>Building materials. Ceramics. Glasses</topic><topic>Ceramic industries</topic><topic>Ceramics</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical industry and chemicals</topic><topic>Chemistry and Materials Science</topic><topic>Composites</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Crystallography and Scattering Methods</topic><topic>Electrochemistry</topic><topic>Electrotechnical and electronic ceramics</topic><topic>Exact sciences and technology</topic><topic>Glass</topic><topic>Liquid phase epitaxy; deposition from liquid phases (melts, solutions, and surface layers on liquids)</topic><topic>Materials Science</topic><topic>Methods of deposition of films and coatings; film growth and epitaxy</topic><topic>Natural Materials</topic><topic>Optical and Electronic Materials</topic><topic>Palladium</topic><topic>Physics</topic><topic>Scanning electron microscopy</topic><topic>Screen printing</topic><topic>Silver</topic><topic>Sol gel process</topic><topic>Spin coating</topic><topic>Technical ceramics</topic><topic>Thick films</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhang, Hongfang</creatorcontrib><creatorcontrib>Zhang, Liangying</creatorcontrib><creatorcontrib>Yao, Xi</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Aluminium Industry Abstracts</collection><jtitle>Journal of electroceramics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhang, Hongfang</au><au>Zhang, Liangying</au><au>Yao, Xi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Fabrication and electrical properties of barium strontium titanate thick films by modified sol–gel method</atitle><jtitle>Journal of electroceramics</jtitle><stitle>J Electroceram</stitle><date>2008-12-01</date><risdate>2008</risdate><volume>21</volume><issue>1-4</issue><spage>503</spage><epage>507</epage><pages>503-507</pages><issn>1385-3449</issn><eissn>1573-8663</eissn><coden>JOELFJ</coden><abstract>A modified sol–gel method has been developed to prepare for the barium strontium titanate (Ba
0.6
Sr
0.4
TiO
3
, BST) thick films. The films were deposited on either Pd–Ag electroded alumina substrates (Pd–Ag/Al
2
O
3
) or silver electroded alumina (Ag/Al
2
O
3
) substrates by spin coating technique or screen printing technique. The thickness of the film was in the range of 2–10 μm. The key point of the process is to disperse fine-grained BST ceramic powders prepared by high energy ball mill into BST sol solution to form a slurry for spin coating and screen printing. In order to enhance the stability of the slurry and to avoid crack formation of the thick film, organic macromolecular poly-vinylpyrrolidone (PVP) was added to the sol solution. The structure and surface morphology of the films were studied by X-ray diffraction and Scanning Electron Microscope (SEM) techniques. It is revealed that the thick films exhibit pure perovskite phase and are crack-free, dense and homogeneous. The dielectric constant and loss tangent of the thick films are about 1200 and 0.01, at 10 °C and 1 KHz, respectively.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1007/s10832-007-9229-9</doi><tpages>5</tpages></addata></record> |
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subjects | Aluminum oxide Applied sciences Barium strontium titanates Building materials. Ceramics. Glasses Ceramic industries Ceramics Characterization and Evaluation of Materials Chemical industry and chemicals Chemistry and Materials Science Composites Cross-disciplinary physics: materials science rheology Crystallography and Scattering Methods Electrochemistry Electrotechnical and electronic ceramics Exact sciences and technology Glass Liquid phase epitaxy deposition from liquid phases (melts, solutions, and surface layers on liquids) Materials Science Methods of deposition of films and coatings film growth and epitaxy Natural Materials Optical and Electronic Materials Palladium Physics Scanning electron microscopy Screen printing Silver Sol gel process Spin coating Technical ceramics Thick films |
title | Fabrication and electrical properties of barium strontium titanate thick films by modified sol–gel method |
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