Characterization of sampling behavior for multielements in NIST SRM 2703

Sampling behavior of multielements for NIST SRM 2703, a marine sediment, was studied with sample sizes from 1 mg down to ng level by a combination of INAA, PIXE and SRXRF. On 1 mg sample size level, sampling behavior for multielements in NIST SRM 2703 and its parent SRM 2702 were comparatively chara...

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Veröffentlicht in:Journal of radioanalytical and nuclear chemistry 2011-04, Vol.288 (1), p.163-169
Hauptverfasser: Donghui, Huang, Hongchao, Sun, Bangfa, Ni, Weizhi, Tian, Yuanxun, Zhang, Pingsheng, Wang, CunXiong, Liu, Guiying, Zhang, Caijin, Xiao, Haiqing, Zhang, Changjun, Zhao
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Sprache:eng
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Zusammenfassung:Sampling behavior of multielements for NIST SRM 2703, a marine sediment, was studied with sample sizes from 1 mg down to ng level by a combination of INAA, PIXE and SRXRF. On 1 mg sample size level, sampling behavior for multielements in NIST SRM 2703 and its parent SRM 2702 were comparatively characterized by using INAA combining with Ingamells model. Results showed that sampling uncertainties for 12 elements of both materials were found to be better than 1%, and those of four other elements in SRM 2703 better than in SRM 2702. At sample sizes not able to be accurately weighed (
ISSN:0236-5731
1588-2780
DOI:10.1007/s10967-010-0910-0