Synthesis and complete assignment of NMR data of 20 chalcones
Chalcones, intermediates in flavonoid biosynthesis, can exhibit antibacterial, antiproliferative, and anti‐inflammatory properties. Chalcones contain two benzene rings and both hydroxylated and methoxylated analogs are frequently produced by hydroxylases and O‐methyltransferases in plant biosyntheti...
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| Veröffentlicht in: | Magnetic resonance in chemistry 2011-01, Vol.49 (1), p.41-45 |
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| creator | Hwang, Doseok Hyun, Jiye Jo, Geunhyeong Koh, Dongsoo Lim, Yoongho |
| description | Chalcones, intermediates in flavonoid biosynthesis, can exhibit antibacterial, antiproliferative, and anti‐inflammatory properties. Chalcones contain two benzene rings and both hydroxylated and methoxylated analogs are frequently produced by hydroxylases and O‐methyltransferases in plant biosynthetic pathways. Assignments of NMR peaks in the spectra of hydroxylated and/or methoxylated chalcones can help in identifying novel chalcone derivatives isolated from natural sources by referencing these data against NMR spectra obtained from known chalcones. We report here the syntheses of 20 chalcones and complete assignments of 1H and 13C NMR spectra. Copyright © 2010 John Wiley & Sons, Ltd.
Chalcones, intermediates in flavonoid biosyntheses, can exhibit antibacterial, antiproliferative, and anti‐inflammatory properties. Assignments of NMR peaks in the spectra of hydroxylated and/or methoxylated chalcones can help in identifying novel chalcone derivatives isolated from natural sources by referencing these data against NMR spectra obtained from known chalcones. We report here the syntheses of 20 chalcones and complete assignments of 1H and 13C NMR spectra. |
| doi_str_mv | 10.1002/mrc.2707 |
| format | Article |
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Chalcones, intermediates in flavonoid biosyntheses, can exhibit antibacterial, antiproliferative, and anti‐inflammatory properties. Assignments of NMR peaks in the spectra of hydroxylated and/or methoxylated chalcones can help in identifying novel chalcone derivatives isolated from natural sources by referencing these data against NMR spectra obtained from known chalcones. We report here the syntheses of 20 chalcones and complete assignments of 1H and 13C NMR spectra.</description><identifier>ISSN: 0749-1581</identifier><identifier>ISSN: 1097-458X</identifier><identifier>EISSN: 1097-458X</identifier><identifier>DOI: 10.1002/mrc.2707</identifier><identifier>PMID: 21113969</identifier><language>eng</language><publisher>Chichester, UK: John Wiley & Sons, Ltd</publisher><subject>13C NMR ; 1H NMR ; 2D NMR ; Antiproliferatives ; Benzene ; Carbon Isotopes ; chalcone ; Chalcones - chemical synthesis ; Chalcones - chemistry ; Derivatives ; flavonoid ; Flavonoids ; Magnetic Resonance Spectroscopy - standards ; Molecular Structure ; NMR ; Nuclear magnetic resonance ; Protons ; Reference Standards ; Referencing ; Spectra ; Stereoisomerism ; Synthesis</subject><ispartof>Magnetic resonance in chemistry, 2011-01, Vol.49 (1), p.41-45</ispartof><rights>Copyright © 2010 John Wiley & Sons, Ltd.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4237-f72c98bb2aba6b26c2cd4d2ca3d960a46137f5ce7bd5bf7f99b954402ad3c9ed3</citedby><cites>FETCH-LOGICAL-c4237-f72c98bb2aba6b26c2cd4d2ca3d960a46137f5ce7bd5bf7f99b954402ad3c9ed3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fmrc.2707$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fmrc.2707$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/21113969$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Hwang, Doseok</creatorcontrib><creatorcontrib>Hyun, Jiye</creatorcontrib><creatorcontrib>Jo, Geunhyeong</creatorcontrib><creatorcontrib>Koh, Dongsoo</creatorcontrib><creatorcontrib>Lim, Yoongho</creatorcontrib><title>Synthesis and complete assignment of NMR data of 20 chalcones</title><title>Magnetic resonance in chemistry</title><addtitle>Magn. Reson. Chem</addtitle><description>Chalcones, intermediates in flavonoid biosynthesis, can exhibit antibacterial, antiproliferative, and anti‐inflammatory properties. Chalcones contain two benzene rings and both hydroxylated and methoxylated analogs are frequently produced by hydroxylases and O‐methyltransferases in plant biosynthetic pathways. Assignments of NMR peaks in the spectra of hydroxylated and/or methoxylated chalcones can help in identifying novel chalcone derivatives isolated from natural sources by referencing these data against NMR spectra obtained from known chalcones. We report here the syntheses of 20 chalcones and complete assignments of 1H and 13C NMR spectra. Copyright © 2010 John Wiley & Sons, Ltd.
Chalcones, intermediates in flavonoid biosyntheses, can exhibit antibacterial, antiproliferative, and anti‐inflammatory properties. Assignments of NMR peaks in the spectra of hydroxylated and/or methoxylated chalcones can help in identifying novel chalcone derivatives isolated from natural sources by referencing these data against NMR spectra obtained from known chalcones. We report here the syntheses of 20 chalcones and complete assignments of 1H and 13C NMR spectra.</description><subject>13C NMR</subject><subject>1H NMR</subject><subject>2D NMR</subject><subject>Antiproliferatives</subject><subject>Benzene</subject><subject>Carbon Isotopes</subject><subject>chalcone</subject><subject>Chalcones - chemical synthesis</subject><subject>Chalcones - chemistry</subject><subject>Derivatives</subject><subject>flavonoid</subject><subject>Flavonoids</subject><subject>Magnetic Resonance Spectroscopy - standards</subject><subject>Molecular Structure</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Protons</subject><subject>Reference Standards</subject><subject>Referencing</subject><subject>Spectra</subject><subject>Stereoisomerism</subject><subject>Synthesis</subject><issn>0749-1581</issn><issn>1097-458X</issn><issn>1097-458X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqF0ctOwkAUBuCJ0QiiiU9gutNNcS7tTGfhQomiBjCCRneTuVWqvWCnRHl721Bxpa7OWXz5T3J-AA4R7CMI8WlW6j5mkG2BLoKc-UEYPW-DLmQB91EYoQ7Yc-4VQsg5I7uggxFChFPeBWezVV7NrUucJ3Pj6SJbpLaynnQueckzm1deEXuT8dQzspLNjqGn5zLVRW7dPtiJZersQTt74PHq8mFw7Y_uhjeD85GvA0yYHzOseaQUlkpShanG2gQGa0kMp1AGFBEWh9oyZUIVs5hzxcMggFgaork1pAeO17mLsnhfWleJLHHapqnMbbF0gkNE65D62H8yQhFt7pFanvwpEaMYYYZD-EN1WThX2lgsyiST5UogKJoCRF2AaAqo6VGbulSZNRv4_fEa-GvwkaR29WuQGE8HbWDrE1fZz42X5ZugjLBQPE2G4uJ2hqN7ikVEvgARApwu</recordid><startdate>201101</startdate><enddate>201101</enddate><creator>Hwang, Doseok</creator><creator>Hyun, Jiye</creator><creator>Jo, Geunhyeong</creator><creator>Koh, Dongsoo</creator><creator>Lim, Yoongho</creator><general>John Wiley & Sons, Ltd</general><scope>BSCLL</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>7X8</scope></search><sort><creationdate>201101</creationdate><title>Synthesis and complete assignment of NMR data of 20 chalcones</title><author>Hwang, Doseok ; Hyun, Jiye ; Jo, Geunhyeong ; Koh, Dongsoo ; Lim, Yoongho</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4237-f72c98bb2aba6b26c2cd4d2ca3d960a46137f5ce7bd5bf7f99b954402ad3c9ed3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>13C NMR</topic><topic>1H NMR</topic><topic>2D NMR</topic><topic>Antiproliferatives</topic><topic>Benzene</topic><topic>Carbon Isotopes</topic><topic>chalcone</topic><topic>Chalcones - chemical synthesis</topic><topic>Chalcones - chemistry</topic><topic>Derivatives</topic><topic>flavonoid</topic><topic>Flavonoids</topic><topic>Magnetic Resonance Spectroscopy - standards</topic><topic>Molecular Structure</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Protons</topic><topic>Reference Standards</topic><topic>Referencing</topic><topic>Spectra</topic><topic>Stereoisomerism</topic><topic>Synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hwang, Doseok</creatorcontrib><creatorcontrib>Hyun, Jiye</creatorcontrib><creatorcontrib>Jo, Geunhyeong</creatorcontrib><creatorcontrib>Koh, Dongsoo</creatorcontrib><creatorcontrib>Lim, Yoongho</creatorcontrib><collection>Istex</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><jtitle>Magnetic resonance in chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hwang, Doseok</au><au>Hyun, Jiye</au><au>Jo, Geunhyeong</au><au>Koh, Dongsoo</au><au>Lim, Yoongho</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and complete assignment of NMR data of 20 chalcones</atitle><jtitle>Magnetic resonance in chemistry</jtitle><addtitle>Magn. Reson. Chem</addtitle><date>2011-01</date><risdate>2011</risdate><volume>49</volume><issue>1</issue><spage>41</spage><epage>45</epage><pages>41-45</pages><issn>0749-1581</issn><issn>1097-458X</issn><eissn>1097-458X</eissn><abstract>Chalcones, intermediates in flavonoid biosynthesis, can exhibit antibacterial, antiproliferative, and anti‐inflammatory properties. Chalcones contain two benzene rings and both hydroxylated and methoxylated analogs are frequently produced by hydroxylases and O‐methyltransferases in plant biosynthetic pathways. Assignments of NMR peaks in the spectra of hydroxylated and/or methoxylated chalcones can help in identifying novel chalcone derivatives isolated from natural sources by referencing these data against NMR spectra obtained from known chalcones. We report here the syntheses of 20 chalcones and complete assignments of 1H and 13C NMR spectra. Copyright © 2010 John Wiley & Sons, Ltd.
Chalcones, intermediates in flavonoid biosyntheses, can exhibit antibacterial, antiproliferative, and anti‐inflammatory properties. Assignments of NMR peaks in the spectra of hydroxylated and/or methoxylated chalcones can help in identifying novel chalcone derivatives isolated from natural sources by referencing these data against NMR spectra obtained from known chalcones. We report here the syntheses of 20 chalcones and complete assignments of 1H and 13C NMR spectra.</abstract><cop>Chichester, UK</cop><pub>John Wiley & Sons, Ltd</pub><pmid>21113969</pmid><doi>10.1002/mrc.2707</doi><tpages>5</tpages></addata></record> |
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| subjects | 13C NMR 1H NMR 2D NMR Antiproliferatives Benzene Carbon Isotopes chalcone Chalcones - chemical synthesis Chalcones - chemistry Derivatives flavonoid Flavonoids Magnetic Resonance Spectroscopy - standards Molecular Structure NMR Nuclear magnetic resonance Protons Reference Standards Referencing Spectra Stereoisomerism Synthesis |
| title | Synthesis and complete assignment of NMR data of 20 chalcones |
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