HRTEM study of oxide nanoparticles in K3-ODS ferritic steel developed for radiation tolerance

Crystal and interfacial structures of oxide nanoparticles and radiation damage in 16Cr–4.5Al–0.3Ti–2W–0.37 Y 2O 3 ODS ferritic steel have been examined using high-resolution transmission electron microscopy (HRTEM) techniques. Oxide nanoparticles with a complex-oxide core and an amorphous shell were...

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Veröffentlicht in:Journal of nuclear materials 2011-02, Vol.409 (2), p.72-79
Hauptverfasser: Hsiung, L., Fluss, M., Tumey, S., Kuntz, J., El-Dasher, B., Wall, M., Choi, B., Kimura, A., Willaime, F., Serruys, Y.
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Sprache:eng
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Zusammenfassung:Crystal and interfacial structures of oxide nanoparticles and radiation damage in 16Cr–4.5Al–0.3Ti–2W–0.37 Y 2O 3 ODS ferritic steel have been examined using high-resolution transmission electron microscopy (HRTEM) techniques. Oxide nanoparticles with a complex-oxide core and an amorphous shell were frequently observed. The crystal structure of complex-oxide core is identified to be mainly monoclinic Y 4Al 2O 9 (YAM) oxide compound. Orientation relationships between the oxide and the matrix are found to be dependent on the particle size. Large particles (>20 nm) tend to be incoherent and have a spherical shape, whereas small particles (
ISSN:0022-3115
1873-4820
DOI:10.1016/j.jnucmat.2010.09.014