Borrowing Hydrogen Methodology for Amine Synthesis under Solvent-Free Microwave Conditions

Borrowing Hydrogen Methodology for Amine Synthesis under Solvent-Free Microwave Conditions

Application of microwave heating to the Borrowing Hydrogen strategy to form C−N bonds from alcohols and amines is presented, removing the need for solvent and reducing the reaction times while still yielding results comparable with those using thermal heating.

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Veröffentlicht in:Journal of organic chemistry 2011-04, Vol.76 (7), p.2328-2331
Hauptverfasser: Watson, Andrew J. A, Maxwell, Aoife C, Williams, Jonathan M. J
Format: Artikel
Sprache:eng
Schlagworte:
Alcohols - chemistry
Aliphatic compounds
Amines - chemical synthesis
Amines - chemistry
Catalysis
Catalysts: preparations and properties
Chemistry
Exact sciences and technology
General and physical chemistry
Heating
Hydrogen - chemistry
Microwaves
Molecular Structure
Organic chemistry
Preparations and properties
Solvents - chemistry
Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry
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Beschreibung
Zusammenfassung:Application of microwave heating to the Borrowing Hydrogen strategy to form C−N bonds from alcohols and amines is presented, removing the need for solvent and reducing the reaction times while still yielding results comparable with those using thermal heating.
ISSN:0022-3263
1520-6904
DOI:10.1021/jo102521a