Thermal dehydration of steroidal allylic alcohols

Thermal dehydration of steroidal allylic alcohols

The direct thermal elimination of water and acetic acid, from the epimeric cholest-4-en-3-ols and their acetates, in the gas Chromatograph yields a mixture of homoannular and heteroannular dienes. Evidence for the structures proposed was obtained after separation and characterization by means of U.V...

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Veröffentlicht in:Steroids 1968-09, Vol.12 (3), p.435-443
Hauptverfasser: Okerholm, Richard A., Brecher, Peter I., Wotiz, Herbert H.
Format: Artikel
Sprache:eng
Schlagworte:
Alcohols
Cholestanes
Chromatography
Hot Temperature
Spectrum Analysis
Water
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Zusammenfassung:The direct thermal elimination of water and acetic acid, from the epimeric cholest-4-en-3-ols and their acetates, in the gas Chromatograph yields a mixture of homoannular and heteroannular dienes. Evidence for the structures proposed was obtained after separation and characterization by means of U.V. and Mass Spectroscopy.
ISSN:0039-128X
1878-5867
DOI:10.1016/0039-128X(68)90033-0