Transmission electron microscopy study of defects in AlN crystals with rough and smooth surface grains

Defects present in (0 0 0 1) textured polycrystalline AlN grown by the sublimation–recombination method were analyzed using transmission electron microscopy (TEM) methods. Grains in the polycrystalline boule had either a smooth or a rough surface. The rough surface grains had mainly edge dislocation...

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Veröffentlicht in:Journal of crystal growth 2010-11, Vol.312 (23), p.3479-3484
Hauptverfasser: Nyakiti, L.O., Chaudhuri, J., Gu, Z., Edgar, J.H.
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container_title Journal of crystal growth
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creator Nyakiti, L.O.
Chaudhuri, J.
Gu, Z.
Edgar, J.H.
description Defects present in (0 0 0 1) textured polycrystalline AlN grown by the sublimation–recombination method were analyzed using transmission electron microscopy (TEM) methods. Grains in the polycrystalline boule had either a smooth or a rough surface. The rough surface grains had mainly edge dislocations, whereas the smooth surface grains had some sub-grain boundaries and were mostly free of dislocations. Dislocations at the grain boundaries were pinned and could not be annihilated.
doi_str_mv 10.1016/j.jcrysgro.2010.09.014
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subjects A1. Dislocations
A1. Grain boundaries
A1. Polarity
A1. Transmission electron microscopy
A3. Sublimation–recombination crystal growth
Aluminum nitride
B1. Aluminum nitride
Boundaries
Condensed matter: structure, mechanical and thermal properties
Cross-disciplinary physics: materials science
rheology
Crystal defects
Crystal growth
Defects and impurities in crystals
microstructure
Dislocations
Electron microscopy
Exact sciences and technology
Grain and twin boundaries
Grain boundaries
Grains
Growth from vapor
Materials science
Methods of crystal growth
physics of crystal growth
Physics
Structure of solids and liquids
crystallography
title Transmission electron microscopy study of defects in AlN crystals with rough and smooth surface grains
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