Hydroxyapatite spheres with controlled porosity for eye ball prosthesis: processing and characterization

Porous hydroxyapatite spheres were prepared by a modified gelcasting method producing a ceramic prosthesis with controled porosity. The spheres are approximately 2.2 cm in diameter with a relatively homogeneous pore size distribution from 10 to 40 microm in diameter. The samples were characterized by X-ray powder diffractometry (XRD) and Fourier transform infra-red spectroscopy (FTIR) to identify the phases both prior to and after the gelcasting process. Surface morphology analysis and porosity evaluations were performed with scanning electron microscopy (SEM), while surface area measurements were carried out by the BET technique.