Nuclear Magnetic Resonance Studies of Cytochalasin E and Its Decomposition Product
The proton and carbon-13 nuclear magnetic resonance signals of cytochalasin E (1) were assigned with the aid of 1H-1H, 1H-13C and 1H-13C long-range chemical shift correlation spectroscopy spectra, and the structure of the decomposition product (2) generated under neutral conditions was determined.
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| Veröffentlicht in: | Chemical & pharmaceutical bulletin 1989/08/25, Vol.37(8), pp.2212-2213 |
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| container_end_page | 2213 |
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| container_issue | 8 |
| container_start_page | 2212 |
| container_title | Chemical & pharmaceutical bulletin |
| container_volume | 37 |
| creator | KAJIMOTO, Tetsuya IMAMURA, Yohko YAMASHITA, Masami TAKAHASHI, Kokichi SHIBATA, Motoo NOHARA, Toshihiro |
| description | The proton and carbon-13 nuclear magnetic resonance signals of cytochalasin E (1) were assigned with the aid of 1H-1H, 1H-13C and 1H-13C long-range chemical shift correlation spectroscopy spectra, and the structure of the decomposition product (2) generated under neutral conditions was determined. |
| doi_str_mv | 10.1248/cpb.37.2212 |
| format | Article |
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Pharm. Bull.</addtitle><description>The proton and carbon-13 nuclear magnetic resonance signals of cytochalasin E (1) were assigned with the aid of 1H-1H, 1H-13C and 1H-13C long-range chemical shift correlation spectroscopy spectra, and the structure of the decomposition product (2) generated under neutral conditions was determined.</description><subject>1H-13C long-range COSY spectrum</subject><subject>Analytical, structural and metabolic biochemistry</subject><subject>Biological and medical sciences</subject><subject>cytochalasin E</subject><subject>Cytochalasins - analysis</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Intermediary metabolites. Miscellaneous</subject><subject>Magnetic Resonance Spectroscopy</subject><subject>Other biological molecules</subject><subject>phytopathogenic fungus</subject><subject>Rosellinia necatrix</subject><subject>X-Ray Diffraction</subject><subject>Xylariales - analysis</subject><issn>0009-2363</issn><issn>1347-5223</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1989</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNpdkUFv1DAQRi0EKsvCiTOSJRAXlMX2xLFzRNtCK7UFFThbE8dus8rGW9s59N-TaKOtxGV8-J7mGz0T8p6zDRel_moPzQbURgguXpAVh1IVUgh4SVaMsboQUMFr8ialHWNCMgVn5EzIWoMoV-TudrS9w0hv8H5wubP0zqUw4GAd_Z3HtnOJBk-3TznYB-wxdQO9oDi09Coneu5s2B9C6nIXBvorhna0-S155bFP7t3yrsnf7xd_tpfF9c8fV9tv14WtQOYCOGihXWOFFwqsa7S10nkovZcMy9Iq64WXLQpb115jIwE4R42Kt5IzBmvy-bj3EMPj6FI2-y5Z1_c4uDAmo2rQvFIz-PE_cBfGOEy3GV5WjKtKT-yafDlSNoaUovPmELs9xifDmZk9m8mzAWVmzxP9Ydk5NnvXnthF7JR_WnJMFnsfJ6NdOmFTI3BRTdj5EduljPfulGOcvqJ3cyWvpZ5rlzG3P8cPGI0b4B8vgJyZ</recordid><startdate>1989</startdate><enddate>1989</enddate><creator>KAJIMOTO, Tetsuya</creator><creator>IMAMURA, Yohko</creator><creator>YAMASHITA, Masami</creator><creator>TAKAHASHI, Kokichi</creator><creator>SHIBATA, Motoo</creator><creator>NOHARA, Toshihiro</creator><general>The Pharmaceutical Society of Japan</general><general>Maruzen</general><general>Japan Science and Technology Agency</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7TK</scope><scope>7TM</scope><scope>7U9</scope><scope>H94</scope><scope>7X8</scope></search><sort><creationdate>1989</creationdate><title>Nuclear Magnetic Resonance Studies of Cytochalasin E and Its Decomposition Product</title><author>KAJIMOTO, Tetsuya ; IMAMURA, Yohko ; YAMASHITA, Masami ; TAKAHASHI, Kokichi ; SHIBATA, Motoo ; NOHARA, Toshihiro</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c635t-313828ebc2f273ceb8cc5ef34ff50a44c7cf2f5da2c99f8ab53311a8a71d51003</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1989</creationdate><topic>1H-13C long-range COSY spectrum</topic><topic>Analytical, structural and metabolic biochemistry</topic><topic>Biological and medical sciences</topic><topic>cytochalasin E</topic><topic>Cytochalasins - analysis</topic><topic>Fundamental and applied biological sciences. 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Miscellaneous</topic><topic>Magnetic Resonance Spectroscopy</topic><topic>Other biological molecules</topic><topic>phytopathogenic fungus</topic><topic>Rosellinia necatrix</topic><topic>X-Ray Diffraction</topic><topic>Xylariales - analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>KAJIMOTO, Tetsuya</creatorcontrib><creatorcontrib>IMAMURA, Yohko</creatorcontrib><creatorcontrib>YAMASHITA, Masami</creatorcontrib><creatorcontrib>TAKAHASHI, Kokichi</creatorcontrib><creatorcontrib>SHIBATA, Motoo</creatorcontrib><creatorcontrib>NOHARA, Toshihiro</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Neurosciences Abstracts</collection><collection>Nucleic Acids Abstracts</collection><collection>Virology and AIDS Abstracts</collection><collection>AIDS and Cancer Research Abstracts</collection><collection>MEDLINE - Academic</collection><jtitle>Chemical & pharmaceutical bulletin</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>KAJIMOTO, Tetsuya</au><au>IMAMURA, Yohko</au><au>YAMASHITA, Masami</au><au>TAKAHASHI, Kokichi</au><au>SHIBATA, Motoo</au><au>NOHARA, Toshihiro</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Nuclear Magnetic Resonance Studies of Cytochalasin E and Its Decomposition Product</atitle><jtitle>Chemical & pharmaceutical bulletin</jtitle><addtitle>Chem. Pharm. Bull.</addtitle><date>1989</date><risdate>1989</risdate><volume>37</volume><issue>8</issue><spage>2212</spage><epage>2213</epage><pages>2212-2213</pages><issn>0009-2363</issn><eissn>1347-5223</eissn><coden>CPBTAL</coden><abstract>The proton and carbon-13 nuclear magnetic resonance signals of cytochalasin E (1) were assigned with the aid of 1H-1H, 1H-13C and 1H-13C long-range chemical shift correlation spectroscopy spectra, and the structure of the decomposition product (2) generated under neutral conditions was determined.</abstract><cop>Tokyo</cop><pub>The Pharmaceutical Society of Japan</pub><pmid>2598324</pmid><doi>10.1248/cpb.37.2212</doi><tpages>2</tpages><oa>free_for_read</oa></addata></record> |
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| identifier | ISSN: 0009-2363 |
| ispartof | Chemical and Pharmaceutical Bulletin, 1989/08/25, Vol.37(8), pp.2212-2213 |
| issn | 0009-2363 1347-5223 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_79381670 |
| source | J-STAGE Free; MEDLINE; EZB-FREE-00999 freely available EZB journals; Free Full-Text Journals in Chemistry |
| subjects | 1H-13C long-range COSY spectrum Analytical, structural and metabolic biochemistry Biological and medical sciences cytochalasin E Cytochalasins - analysis Fundamental and applied biological sciences. Psychology Intermediary metabolites. Miscellaneous Magnetic Resonance Spectroscopy Other biological molecules phytopathogenic fungus Rosellinia necatrix X-Ray Diffraction Xylariales - analysis |
| title | Nuclear Magnetic Resonance Studies of Cytochalasin E and Its Decomposition Product |
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