Nuclear Magnetic Resonance Studies of Cytochalasin E and Its Decomposition Product

The proton and carbon-13 nuclear magnetic resonance signals of cytochalasin E (1) were assigned with the aid of 1H-1H, 1H-13C and 1H-13C long-range chemical shift correlation spectroscopy spectra, and the structure of the decomposition product (2) generated under neutral conditions was determined.

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Veröffentlicht in:Chemical & pharmaceutical bulletin 1989/08/25, Vol.37(8), pp.2212-2213
Hauptverfasser: KAJIMOTO, Tetsuya, IMAMURA, Yohko, YAMASHITA, Masami, TAKAHASHI, Kokichi, SHIBATA, Motoo, NOHARA, Toshihiro
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Sprache:eng
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Zusammenfassung:The proton and carbon-13 nuclear magnetic resonance signals of cytochalasin E (1) were assigned with the aid of 1H-1H, 1H-13C and 1H-13C long-range chemical shift correlation spectroscopy spectra, and the structure of the decomposition product (2) generated under neutral conditions was determined.
ISSN:0009-2363
1347-5223
DOI:10.1248/cpb.37.2212