Energy resolution of an Omega-type monochromator and imaging properties of the MANDOLINE filter
We report on the energy resolution properties of an Omega-type monochromator. In a TEM/STEM setup with a MANDOLINE filter and extreme stability of the high voltage and the filter current, an energy resolution of 43 meV for 0.1 s exposure time and 87 meV for 100 s exposure time was measured at 200 kV...
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Veröffentlicht in: | Ultramicroscopy 2010-07, Vol.110 (8), p.971-980 |
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Hauptverfasser: | , , , , , , |
Format: | Artikel |
Sprache: | eng |
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Zusammenfassung: | We report on the energy resolution properties of an Omega-type monochromator. In a TEM/STEM setup with a MANDOLINE filter and extreme stability of the high voltage and the filter current, an energy resolution of 43
meV for 0.1
s exposure time and 87
meV for 100
s exposure time was measured at 200
kV with 40
meV monochromator slit width. The monochromized zero-loss peaks are additionally characterized by their edge steepness. Moreover a drop in the monochromized zero-loss peak by 10
3 after 260
meV can be obtained even without deconvolution. For small fields of view, the energy resolution mostly does not depend on the MANDOLINE filter. With the Corrected OMEGA filter an energy resolution of 41
meV was measured for 0.03
s exposure time at 200
kV with 30
meV monochromator slit width and 77
meV for 50
s exposure time at 80
kV with 40
meV monochromator slit width. Furthermore, the MANDOLINE filter’s setup and imaging properties are presented such as isochromaticity ( |
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ISSN: | 0304-3991 1879-2723 |
DOI: | 10.1016/j.ultramic.2010.02.009 |