High Performance Liquid Chromatography Assay for Piroxicam in Pharmaceutical Products
A high performance liquid chromatographic assay for piroxicam in pharmaceutical preparations is described. The method uses a reversed-phase C18 column with pH 3 aqueous buffer/methanol, 55:45, v/v mobile phase, and is selective for piroxicam in the presence of other “oxicams,” synthetic precursors,...
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| Veröffentlicht in: | Journal of chromatographic science 1987-07, Vol.25 (7), p.292-295 |
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| container_end_page | 295 |
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| container_issue | 7 |
| container_start_page | 292 |
| container_title | Journal of chromatographic science |
| container_volume | 25 |
| creator | Richards, Jeffrey A. Cole, Dale A. Hickey, Robert J. Sokol, Lucia S-W. |
| description | A high performance liquid chromatographic assay for piroxicam in pharmaceutical preparations is described. The method uses a reversed-phase C18 column with pH 3 aqueous buffer/methanol, 55:45, v/v mobile phase, and is selective for piroxicam in the presence of other “oxicams,” synthetic precursors, by-products, degradation products, metabolites, and related compounds. Applications to capsules, tablets, ointments, suppositories, ophthalmic suspensions, and rodent feeds are cited. |
| doi_str_mv | 10.1093/chromsci/25.7.292 |
| format | Article |
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The method uses a reversed-phase C18 column with pH 3 aqueous buffer/methanol, 55:45, v/v mobile phase, and is selective for piroxicam in the presence of other “oxicams,” synthetic precursors, by-products, degradation products, metabolites, and related compounds. Applications to capsules, tablets, ointments, suppositories, ophthalmic suspensions, and rodent feeds are cited.</description><identifier>ISSN: 0021-9665</identifier><identifier>EISSN: 1945-239X</identifier><identifier>DOI: 10.1093/chromsci/25.7.292</identifier><identifier>PMID: 3611284</identifier><identifier>CODEN: JCHSBZ</identifier><language>eng</language><publisher>Niles, IL: Oxford University Press</publisher><subject>Animal Feed - analysis ; Biological and medical sciences ; Bones, joints and connective tissue. Antiinflammatory agents ; Capsules ; Chromatography, High Pressure Liquid ; Drug Stability ; Hydrogen-Ion Concentration ; Medical sciences ; Ointments ; Ophthalmic Solutions ; Pharmacology. 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The method uses a reversed-phase C18 column with pH 3 aqueous buffer/methanol, 55:45, v/v mobile phase, and is selective for piroxicam in the presence of other “oxicams,” synthetic precursors, by-products, degradation products, metabolites, and related compounds. Applications to capsules, tablets, ointments, suppositories, ophthalmic suspensions, and rodent feeds are cited.</description><subject>Animal Feed - analysis</subject><subject>Biological and medical sciences</subject><subject>Bones, joints and connective tissue. Antiinflammatory agents</subject><subject>Capsules</subject><subject>Chromatography, High Pressure Liquid</subject><subject>Drug Stability</subject><subject>Hydrogen-Ion Concentration</subject><subject>Medical sciences</subject><subject>Ointments</subject><subject>Ophthalmic Solutions</subject><subject>Pharmacology. Drug treatments</subject><subject>Piroxicam - administration & dosage</subject><subject>Piroxicam - analysis</subject><subject>Spectrophotometry, Ultraviolet</subject><subject>Suppositories</subject><issn>0021-9665</issn><issn>1945-239X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1987</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNo9kMFPwjAYxRujQUT_AA8mPRhvg7Vd2_VIiIoJiRzEEC5N13Wsyhi0WwL_vSVMTl--7_3ea_oAeETxEMWCjHTp6sprO8J0yIdY4CvQRyKhESZieQ36cYxRJBijt-DO-5_TilLaAz3CEMJp0geLqV2XcG5cUbtKbbWBM7tvbQ4np2jV1GunduURjr1XRxggOLeuPlitKmi3cF6qYNOmbcJlA-euzlvd-HtwU6iNNw_dHIDF2-vXZBrNPt8_JuNZpAkjTYQLhlFmVCzygvJEZbkqqMiThJqEGcUY4kaYcEXEZASnNMk0w4LmKSZUI04G4OWcu3P1vjW-kZX12mw2amvq1kvOGcI0QQFEZ1C72ntnCrlztlLuKFEsT1XK_yolppLLUGXwPHXhbVaZ_OLougv6c6crHz5fuFCf9RcsPJ2yVAQsOmPWN-ZwkZX7lYwTTuV0uZLfnOMVX62kIH9A5Y64</recordid><startdate>19870701</startdate><enddate>19870701</enddate><creator>Richards, Jeffrey A.</creator><creator>Cole, Dale A.</creator><creator>Hickey, Robert J.</creator><creator>Sokol, Lucia S-W.</creator><general>Oxford University Press</general><general>Preston Publications</general><scope>BSCLL</scope><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>19870701</creationdate><title>High Performance Liquid Chromatography Assay for Piroxicam in Pharmaceutical Products</title><author>Richards, Jeffrey A. ; Cole, Dale A. ; Hickey, Robert J. ; Sokol, Lucia S-W.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c363t-2f621bea09df574abdaf59d445e46ea6617e9ebda13eb32854bc6295d8235c173</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1987</creationdate><topic>Animal Feed - analysis</topic><topic>Biological and medical sciences</topic><topic>Bones, joints and connective tissue. Antiinflammatory agents</topic><topic>Capsules</topic><topic>Chromatography, High Pressure Liquid</topic><topic>Drug Stability</topic><topic>Hydrogen-Ion Concentration</topic><topic>Medical sciences</topic><topic>Ointments</topic><topic>Ophthalmic Solutions</topic><topic>Pharmacology. Drug treatments</topic><topic>Piroxicam - administration & dosage</topic><topic>Piroxicam - analysis</topic><topic>Spectrophotometry, Ultraviolet</topic><topic>Suppositories</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Richards, Jeffrey A.</creatorcontrib><creatorcontrib>Cole, Dale A.</creatorcontrib><creatorcontrib>Hickey, Robert J.</creatorcontrib><creatorcontrib>Sokol, Lucia S-W.</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of chromatographic science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Richards, Jeffrey A.</au><au>Cole, Dale A.</au><au>Hickey, Robert J.</au><au>Sokol, Lucia S-W.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>High Performance Liquid Chromatography Assay for Piroxicam in Pharmaceutical Products</atitle><jtitle>Journal of chromatographic science</jtitle><addtitle>Journal of Chromatographic Science</addtitle><date>1987-07-01</date><risdate>1987</risdate><volume>25</volume><issue>7</issue><spage>292</spage><epage>295</epage><pages>292-295</pages><issn>0021-9665</issn><eissn>1945-239X</eissn><coden>JCHSBZ</coden><abstract>A high performance liquid chromatographic assay for piroxicam in pharmaceutical preparations is described. 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| fulltext | fulltext |
| identifier | ISSN: 0021-9665 |
| ispartof | Journal of chromatographic science, 1987-07, Vol.25 (7), p.292-295 |
| issn | 0021-9665 1945-239X |
| language | eng |
| recordid | cdi_proquest_miscellaneous_77612541 |
| source | MEDLINE; Oxford University Press Journals Digital Archive Legacy |
| subjects | Animal Feed - analysis Biological and medical sciences Bones, joints and connective tissue. Antiinflammatory agents Capsules Chromatography, High Pressure Liquid Drug Stability Hydrogen-Ion Concentration Medical sciences Ointments Ophthalmic Solutions Pharmacology. Drug treatments Piroxicam - administration & dosage Piroxicam - analysis Spectrophotometry, Ultraviolet Suppositories |
| title | High Performance Liquid Chromatography Assay for Piroxicam in Pharmaceutical Products |
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