Isolation and Characterization of All Eight Bisadducts of Fulleropyrrolidine Derivatives

Isolation and Characterization of All Eight Bisadducts of Fulleropyrrolidine Derivatives

We report the isolation and characterization of bisadducts of fulleropyrrolidine derivatives. The compounds were characterized by means of a variety of spectroscopic techniques, including ES-MS, UV−vis, 1H NMR, and 13C NMR. The whole series of bisadducts was separated for the first time in the case...

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Veröffentlicht in:Journal of organic chemistry 2001-04, Vol.66 (8), p.2802-2808
Hauptverfasser: Kordatos, Konstantinos, Bosi, Susanna, Da Ros, Tatiana, Zambon, Alfonso, Lucchini, Vittorio, Prato, Maurizio
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Sprache:eng
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Zusammenfassung:We report the isolation and characterization of bisadducts of fulleropyrrolidine derivatives. The compounds were characterized by means of a variety of spectroscopic techniques, including ES-MS, UV−vis, 1H NMR, and 13C NMR. The whole series of bisadducts was separated for the first time in the case of the bispyrrolidines, and the determination of their structure was obtained by NMR spectroscopy with the help of HMQC and HMBC techniques.
ISSN:0022-3263
1520-6904
DOI:10.1021/jo001708z