Crystal Structure of 2-Selenobenzyl-1-benzoic Acid

C14H12O2Se is monoclinic, P21/c. Unit-cell dimensions at 293 K are a = 8.1055(7), b = 5.8403(11), c = 26.0302(17)Å, β = 94.560(5)°, V = 1228.3(3)Å3, Dx = 1.575 g/cm3, and Z = 4. The R value is 0.048 for 2144 observed reflections. The dihedral angle between the phenyl rings is 74.9(2)°. There is an i...

Ausführliche Beschreibung

Gespeichert in:

Bibliographische Detailangaben
Veröffentlicht in:	Analytical Sciences 2003, Vol.19(9), pp.1349-1350
Hauptverfasser:	RAMOS, Federico Martínez, SORIANO-GARCIíA, Manuel
Format:	Artikel
Sprache:	eng
Schlagworte:	Aliphatic, non-condensed and condensed benzenic, and alicyclic compounds Benzoates - chemistry Condensed matter: structure, mechanical and thermal properties Crystallography, X-Ray Exact sciences and technology Free Radical Scavengers - chemistry Hydrogen Bonding Molecular Structure Organic compounds Physics Selenium Compounds - chemistry Single-crystal and powder diffraction Structure of solids and liquids crystallography Structure of specific crystalline solids X-ray diffraction and scattering
Online-Zugang:	Volltext
Tags:	Tag hinzufügen Keine Tags, Fügen Sie den ersten Tag hinzu!

Beschreibung
Zusammenfassung:	C14H12O2Se is monoclinic, P21/c. Unit-cell dimensions at 293 K are a = 8.1055(7), b = 5.8403(11), c = 26.0302(17)Å, β = 94.560(5)°, V = 1228.3(3)Å3, Dx = 1.575 g/cm3, and Z = 4. The R value is 0.048 for 2144 observed reflections. The dihedral angle between the phenyl rings is 74.9(2)°. There is an intermolecular hydrogen bond between two symmetry related carboxyl groups with an O1···O2 distance of 2.668(6)Å. The molecules in the crystal are packed at normal van der Waals distances.
ISSN:	0910-6340 1348-2246
DOI:	10.2116/analsci.19.1349