Specific Exafs Tools in Analysis of MoSI Nanowires

The structure of nanowires prepared by vapor synthesis from Mo, S and I is investigated by methods of x-ray diffraction (XRD) and extended x-ray absorption fine structure (EXAFS). Starting with a qualitative model of the structure from XRD, the metrics is introduced with interatomic distances determ...

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Veröffentlicht in:Acta chimica Slovenica 2006-01, Vol.53 (1)
Hauptverfasser: Kodre, A, Gomilsek, J P, Arcon, I, Meden, A, Mihailovic, D
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Sprache:eng
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Zusammenfassung:The structure of nanowires prepared by vapor synthesis from Mo, S and I is investigated by methods of x-ray diffraction (XRD) and extended x-ray absorption fine structure (EXAFS). Starting with a qualitative model of the structure from XRD, the metrics is introduced with interatomic distances determined from EXAFS. Two specific tools to increase the resolution of EXAFS method are discussed: the reciprocity relation between data from adjacent target atoms, and difference EXAFS from data on samples with small changes in stoichiometry.
ISSN:1318-0207