Influence of power density and primer application on polymerization of dual-cured resin cements monitored by ultrasonic measurement

Takubo C, Yasuda G, Murayama R, Ogura Y, Tonegawa M, Kurokawa H, Miyazaki M. Influence of power density and primer application on polymerization of dual‐cured resin cements monitored by ultrasonic measurement. Eur J Oral Sci 2010; 118: 417–422. © 2010 The Authors. Journal compilation © 2010 Eur J Oral Sci We used ultrasonic measurements to monitor the influence of power density and primer application on the polymerization reaction of dual‐cured resin cements. The ultrasonic equipment comprised a pulser–receiver, transducers, and an oscilloscope. Resin cements were mixed and inserted into a transparent mould, and specimens were placed on the sample stage, onto which the primer, if used, was also applied. Power densities of 0 (no irradiation), 200, or 600 mW cm−2 were used for curing. The transit time through the cement disk was divided by the specimen thickness to obtain the longitudinal sound velocity. When resin cements were light‐irradiated, each curve displayed an initial plateau of ∼1,500 m s−1, which rapidly increased to a second plateau of 2,300–2,900 m s−1. The rate of sound velocity increase was retarded when the cements were light‐irradiated at lower power densities, and increased when the primer was applied. The polymerization behaviour of dual‐cured resin cements was therefore shown to be affected by the power density of the curing unit and the application of self‐etching primer.