Determination of As(III) and As(V) species in some natural water and food samples by solid-phase extraction on Streptococcus pyogenes immobilized on Sepabeads SP 70 and hydride generation atomic absorption spectrometry
The speciation of arsenic(III) and arsenic(V) by using Streptococcus pyogenes immobilized on Sepabeads SP 70 resin has been investigated with solid-phase extraction method. The arsenic levels were determined hydride generation atomic absorption spectrometry (HGAAS) in sample solutions. The procedure...
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| Veröffentlicht in: | Food and chemical toxicology 2010-05, Vol.48 (5), p.1393-1398 |
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| creator | Uluozlu, Ozgur Dogan Tuzen, Mustafa Mendil, Durali Soylak, Mustafa |
| description | The speciation of arsenic(III) and arsenic(V) by using
Streptococcus pyogenes immobilized on Sepabeads SP 70 resin has been investigated with solid-phase extraction method. The arsenic levels were determined hydride generation atomic absorption spectrometry (HGAAS) in sample solutions. The procedure presented based on quantitative recoveries of As(III) as >95%. Also the As(V) recoveries were obtained as |
| doi_str_mv | 10.1016/j.fct.2010.03.007 |
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Streptococcus pyogenes immobilized on Sepabeads SP 70 resin has been investigated with solid-phase extraction method. The arsenic levels were determined hydride generation atomic absorption spectrometry (HGAAS) in sample solutions. The procedure presented based on quantitative recoveries of As(III) as >95%. Also the As(V) recoveries were obtained as <5% using the presented method. After reduction of As(V) by using KI and ascorbic acid and waiting 1
h later, the system was applied to determination of total arsenic. As(V) was found as the difference between the total As and As(III) content. Various experimental parameters such as pH, amount of microorganism, sample volume, etc. were investigated. The capacity of biosorbent for arsenic(III) was calculated as 7.3
mg/g. The preconcentration factor was found as 36. The relative standard deviation was calculated below 8%. Limit of detection was calculated as 13
ng/L. The validation of the presented procedure was tested by analysis of standard reference materials (NIST SRM 1568a Rice floor and GBW 07605 Tea) and obtained fairly compatible results. The procedure was also successfully applied to arsenic speciation and determination of some natural water and food samples.</description><identifier>ISSN: 0278-6915</identifier><identifier>EISSN: 1873-6351</identifier><identifier>DOI: 10.1016/j.fct.2010.03.007</identifier><identifier>PMID: 20226225</identifier><identifier>CODEN: FCTOD7</identifier><language>eng</language><publisher>Oxford: Elsevier Ltd</publisher><subject>Arsenic ; Arsenic - analysis ; Arsenic - chemistry ; Arsenic - classification ; Arsenicals - analysis ; Arsenicals - chemistry ; Arsenicals - classification ; Atomic absorption analysis ; atomic absorption spectrometry ; Biological and medical sciences ; Carcinogenesis, carcinogens and anticarcinogens ; Chemical agents ; Chemical and industrial products toxicology. Toxic occupational diseases ; chemical speciation ; Extraction ; Food Analysis - methods ; Food Contamination - analysis ; Foods ; Fresh Water - chemistry ; HGAAS ; hydride generation atomic absorption spectrometry ; Hydrides ; immobilized cells ; Ion Exchange Resins - chemistry ; Limit of Detection ; Mathematical analysis ; Medical sciences ; Metals and various inorganic compounds ; model food systems ; Recovery ; Reproducibility of Results ; Sepabeads SP 70 ; Solid Phase Extraction - methods ; Solid-phase extraction ; Speciation ; Spectrophotometry, Atomic ; Streptococcus pyogenes ; Streptococcus pyogenes - chemistry ; Toxicology ; Tumors ; Water Pollutants, Chemical - analysis</subject><ispartof>Food and chemical toxicology, 2010-05, Vol.48 (5), p.1393-1398</ispartof><rights>2010 Elsevier Ltd</rights><rights>2015 INIST-CNRS</rights><rights>Copyright (c) 2010 Elsevier Ltd. All rights reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c438t-761b84cc8629c560dad06f6f217457a7aaba884d61db2d09bd4f4c980be8202f3</citedby><cites>FETCH-LOGICAL-c438t-761b84cc8629c560dad06f6f217457a7aaba884d61db2d09bd4f4c980be8202f3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0278691510001560$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22689416$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/20226225$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Uluozlu, Ozgur Dogan</creatorcontrib><creatorcontrib>Tuzen, Mustafa</creatorcontrib><creatorcontrib>Mendil, Durali</creatorcontrib><creatorcontrib>Soylak, Mustafa</creatorcontrib><title>Determination of As(III) and As(V) species in some natural water and food samples by solid-phase extraction on Streptococcus pyogenes immobilized on Sepabeads SP 70 and hydride generation atomic absorption spectrometry</title><title>Food and chemical toxicology</title><addtitle>Food Chem Toxicol</addtitle><description>The speciation of arsenic(III) and arsenic(V) by using
Streptococcus pyogenes immobilized on Sepabeads SP 70 resin has been investigated with solid-phase extraction method. The arsenic levels were determined hydride generation atomic absorption spectrometry (HGAAS) in sample solutions. The procedure presented based on quantitative recoveries of As(III) as >95%. Also the As(V) recoveries were obtained as <5% using the presented method. After reduction of As(V) by using KI and ascorbic acid and waiting 1
h later, the system was applied to determination of total arsenic. As(V) was found as the difference between the total As and As(III) content. Various experimental parameters such as pH, amount of microorganism, sample volume, etc. were investigated. The capacity of biosorbent for arsenic(III) was calculated as 7.3
mg/g. The preconcentration factor was found as 36. The relative standard deviation was calculated below 8%. Limit of detection was calculated as 13
ng/L. The validation of the presented procedure was tested by analysis of standard reference materials (NIST SRM 1568a Rice floor and GBW 07605 Tea) and obtained fairly compatible results. The procedure was also successfully applied to arsenic speciation and determination of some natural water and food samples.</description><subject>Arsenic</subject><subject>Arsenic - analysis</subject><subject>Arsenic - chemistry</subject><subject>Arsenic - classification</subject><subject>Arsenicals - analysis</subject><subject>Arsenicals - chemistry</subject><subject>Arsenicals - classification</subject><subject>Atomic absorption analysis</subject><subject>atomic absorption spectrometry</subject><subject>Biological and medical sciences</subject><subject>Carcinogenesis, carcinogens and anticarcinogens</subject><subject>Chemical agents</subject><subject>Chemical and industrial products toxicology. Toxic occupational diseases</subject><subject>chemical speciation</subject><subject>Extraction</subject><subject>Food Analysis - methods</subject><subject>Food Contamination - analysis</subject><subject>Foods</subject><subject>Fresh Water - chemistry</subject><subject>HGAAS</subject><subject>hydride generation atomic absorption spectrometry</subject><subject>Hydrides</subject><subject>immobilized cells</subject><subject>Ion Exchange Resins - chemistry</subject><subject>Limit of Detection</subject><subject>Mathematical analysis</subject><subject>Medical sciences</subject><subject>Metals and various inorganic compounds</subject><subject>model food systems</subject><subject>Recovery</subject><subject>Reproducibility of Results</subject><subject>Sepabeads SP 70</subject><subject>Solid Phase Extraction - methods</subject><subject>Solid-phase extraction</subject><subject>Speciation</subject><subject>Spectrophotometry, Atomic</subject><subject>Streptococcus pyogenes</subject><subject>Streptococcus pyogenes - chemistry</subject><subject>Toxicology</subject><subject>Tumors</subject><subject>Water Pollutants, Chemical - analysis</subject><issn>0278-6915</issn><issn>1873-6351</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqF0s1u1DAQB_AIgehSeAAu4AuCHrLYcWJ7xalq-VipEkhLuVoTe9J6lcTBzgLbR-VpcDYL3OAUx_rNeOS_s-wpo0tGmXi9XTZmXBY0_VO-pFTeyxZMSZ4LXrH72YIWUuVixaqT7FGMW5oEk-JhdlLQohBFUS2yn5c4YuhcD6PzPfENOY-v1uv1GYHeTusvZyQOaBxG4noSfYck2V2AlnyHVHpwjfeWROiGNrF6n1jrbD7cQkSCP8YAZu7ek80YcBi98cbsIhn2_gb7qXXX-dq17g7tQeEANYKNZPOJSHo443Zvg7NIpoIwTwuj75whUEcfhsPONOoY0pBj2D_OHjTQRnxy_J5m1-_efr74kF99fL--OL_KTcnVmEvBalUao0SxMpWgFiwVjWgKJstKggSoQanSCmbrwtJVbcumNCtFa1TpHht-mr2c-w7Bf91hHHXnosG2hR79LmpZClZRKfj_JeeCS07LJNksTfAxBmz0EFwHYa8Z1VP2eqtT9nrKXlOuU7Kp5tmx-67u0P6p-B12Ai-OAKKBtgnQGxf_ukKoVclEcs9n14DXcBOSud6kkzhlqpSsUkm8mQWme_3mMOiYXkhv0LqQAtDWu38M-guaqdkf</recordid><startdate>20100501</startdate><enddate>20100501</enddate><creator>Uluozlu, Ozgur Dogan</creator><creator>Tuzen, Mustafa</creator><creator>Mendil, Durali</creator><creator>Soylak, Mustafa</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>FBQ</scope><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope></search><sort><creationdate>20100501</creationdate><title>Determination of As(III) and As(V) species in some natural water and food samples by solid-phase extraction on Streptococcus pyogenes immobilized on Sepabeads SP 70 and hydride generation atomic absorption spectrometry</title><author>Uluozlu, Ozgur Dogan ; Tuzen, Mustafa ; Mendil, Durali ; Soylak, Mustafa</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c438t-761b84cc8629c560dad06f6f217457a7aaba884d61db2d09bd4f4c980be8202f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Arsenic</topic><topic>Arsenic - analysis</topic><topic>Arsenic - chemistry</topic><topic>Arsenic - classification</topic><topic>Arsenicals - analysis</topic><topic>Arsenicals - chemistry</topic><topic>Arsenicals - classification</topic><topic>Atomic absorption analysis</topic><topic>atomic absorption spectrometry</topic><topic>Biological and medical sciences</topic><topic>Carcinogenesis, carcinogens and anticarcinogens</topic><topic>Chemical agents</topic><topic>Chemical and industrial products toxicology. Toxic occupational diseases</topic><topic>chemical speciation</topic><topic>Extraction</topic><topic>Food Analysis - methods</topic><topic>Food Contamination - analysis</topic><topic>Foods</topic><topic>Fresh Water - chemistry</topic><topic>HGAAS</topic><topic>hydride generation atomic absorption spectrometry</topic><topic>Hydrides</topic><topic>immobilized cells</topic><topic>Ion Exchange Resins - chemistry</topic><topic>Limit of Detection</topic><topic>Mathematical analysis</topic><topic>Medical sciences</topic><topic>Metals and various inorganic compounds</topic><topic>model food systems</topic><topic>Recovery</topic><topic>Reproducibility of Results</topic><topic>Sepabeads SP 70</topic><topic>Solid Phase Extraction - methods</topic><topic>Solid-phase extraction</topic><topic>Speciation</topic><topic>Spectrophotometry, Atomic</topic><topic>Streptococcus pyogenes</topic><topic>Streptococcus pyogenes - chemistry</topic><topic>Toxicology</topic><topic>Tumors</topic><topic>Water Pollutants, Chemical - analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Uluozlu, Ozgur Dogan</creatorcontrib><creatorcontrib>Tuzen, Mustafa</creatorcontrib><creatorcontrib>Mendil, Durali</creatorcontrib><creatorcontrib>Soylak, Mustafa</creatorcontrib><collection>AGRIS</collection><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><jtitle>Food and chemical toxicology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Uluozlu, Ozgur Dogan</au><au>Tuzen, Mustafa</au><au>Mendil, Durali</au><au>Soylak, Mustafa</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of As(III) and As(V) species in some natural water and food samples by solid-phase extraction on Streptococcus pyogenes immobilized on Sepabeads SP 70 and hydride generation atomic absorption spectrometry</atitle><jtitle>Food and chemical toxicology</jtitle><addtitle>Food Chem Toxicol</addtitle><date>2010-05-01</date><risdate>2010</risdate><volume>48</volume><issue>5</issue><spage>1393</spage><epage>1398</epage><pages>1393-1398</pages><issn>0278-6915</issn><eissn>1873-6351</eissn><coden>FCTOD7</coden><abstract>The speciation of arsenic(III) and arsenic(V) by using
Streptococcus pyogenes immobilized on Sepabeads SP 70 resin has been investigated with solid-phase extraction method. The arsenic levels were determined hydride generation atomic absorption spectrometry (HGAAS) in sample solutions. The procedure presented based on quantitative recoveries of As(III) as >95%. Also the As(V) recoveries were obtained as <5% using the presented method. After reduction of As(V) by using KI and ascorbic acid and waiting 1
h later, the system was applied to determination of total arsenic. As(V) was found as the difference between the total As and As(III) content. Various experimental parameters such as pH, amount of microorganism, sample volume, etc. were investigated. The capacity of biosorbent for arsenic(III) was calculated as 7.3
mg/g. The preconcentration factor was found as 36. The relative standard deviation was calculated below 8%. Limit of detection was calculated as 13
ng/L. The validation of the presented procedure was tested by analysis of standard reference materials (NIST SRM 1568a Rice floor and GBW 07605 Tea) and obtained fairly compatible results. The procedure was also successfully applied to arsenic speciation and determination of some natural water and food samples.</abstract><cop>Oxford</cop><pub>Elsevier Ltd</pub><pmid>20226225</pmid><doi>10.1016/j.fct.2010.03.007</doi><tpages>6</tpages></addata></record> |
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| subjects | Arsenic Arsenic - analysis Arsenic - chemistry Arsenic - classification Arsenicals - analysis Arsenicals - chemistry Arsenicals - classification Atomic absorption analysis atomic absorption spectrometry Biological and medical sciences Carcinogenesis, carcinogens and anticarcinogens Chemical agents Chemical and industrial products toxicology. Toxic occupational diseases chemical speciation Extraction Food Analysis - methods Food Contamination - analysis Foods Fresh Water - chemistry HGAAS hydride generation atomic absorption spectrometry Hydrides immobilized cells Ion Exchange Resins - chemistry Limit of Detection Mathematical analysis Medical sciences Metals and various inorganic compounds model food systems Recovery Reproducibility of Results Sepabeads SP 70 Solid Phase Extraction - methods Solid-phase extraction Speciation Spectrophotometry, Atomic Streptococcus pyogenes Streptococcus pyogenes - chemistry Toxicology Tumors Water Pollutants, Chemical - analysis |
| title | Determination of As(III) and As(V) species in some natural water and food samples by solid-phase extraction on Streptococcus pyogenes immobilized on Sepabeads SP 70 and hydride generation atomic absorption spectrometry |
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