Determination of arsenic in high-purity copper by flameless atomic-absorption spectrophotometry

Arsenic is separated from an ammoniacal solution containing 1 g or less of copper(II) by co-precipitation with ferric hydroxide. The precipitate is dissolved in nitric acid, the solution almost neutralized with ammonia, made up to volume and the As determined by flameless atomic-absorption spectroph...

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Veröffentlicht in:Talanta (Oxford) 1977-10, Vol.24 (10), p.657-658
1. Verfasser: Mullen, J.D.
Format: Artikel
Sprache:eng
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Zusammenfassung:Arsenic is separated from an ammoniacal solution containing 1 g or less of copper(II) by co-precipitation with ferric hydroxide. The precipitate is dissolved in nitric acid, the solution almost neutralized with ammonia, made up to volume and the As determined by flameless atomic-absorption spectrophotometry. Less than 0.5 ppm can be determined.
ISSN:0039-9140
1873-3573
DOI:10.1016/0039-9140(77)80116-1